(1R)-1-(8-amino-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-O⁵-benzoyl-D-1,4-anhydro-arabinitol

Base Information

• Chemical Name: (1R)-1-(8-amino-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-O⁵-benzoyl-D-1,4-anhydro-arabinitol
• CAS No.: 73012-63-2
• Molecular Formula: C₁₈H₁₈N₄O₅
• Molecular Weight: 370.365

Synonyms:(1R)-1-(8-amino-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-O⁵-benzoyl-D-1,4-anhydro-arabinitol

Chemical Property of (1R)-1-(8-amino-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-O⁵-benzoyl-D-1,4-anhydro-arabinitol

Chemical Property:

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Technology Process of (1R)-1-(8-amino-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-O⁵-benzoyl-D-1,4-anhydro-arabinitol

There total 3 articles about (1R)-1-(8-amino-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-O⁵-benzoyl-D-1,4-anhydro-arabinitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Hydrazino-3-nitropyridine (15367-16-5) → (1R)-1-(8-amino-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-O5-benzoyl-D-1,4-anhydro-arabinitol (73012-63-2)

Guidance literature:

Multi-step reaction with 2 steps

1: Py / Heating

2: H₂ / Pd-C / methanol / Ambient temperature

With pyridine; hydrogen; palladium on activated charcoal; In methanol;

Reference yield:

(1R)-O5-benzoyl-1-(8-nitro-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-D-1,4-anhydro-arabinitol (73012-62-1) → (1R)-1-(8-amino-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-O5-benzoyl-D-1,4-anhydro-arabinitol (73012-63-2)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; Ambient temperature;

Reference yield:

(2Ξ)-O6-benzoyl-D-arabino-2,5-anhydro-hexonimidothioic acid benzyl ester (50908-31-1,50908-32-2,59684-39-8,68779-21-5) → (1R)-1-(8-amino-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-O5-benzoyl-D-1,4-anhydro-arabinitol (73012-63-2)

Guidance literature:

Multi-step reaction with 2 steps

1: Py / Heating

2: H₂ / Pd-C / methanol / Ambient temperature

With pyridine; hydrogen; palladium on activated charcoal; In methanol;

upstream raw materials:

(1R)-O⁵-benzoyl-1-(8-nitro-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-D-1,4-anhydro-arabinitol

(2Ξ)-O⁶-benzoyl-D-arabino-2,5-anhydro-hexonimidothioic acid benzyl ester

2-Hydrazino-3-nitropyridine

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