N-[3-[[[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-(heptafluoro)propyl)phenyl]amino]carbonyl]-2-methoxyphenyl]-4-pyridinecarboxamide

Base Information

Chemical Name:N-[3-[[[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-(heptafluoro)propyl)phenyl]amino]carbonyl]-2-methoxyphenyl]-4-pyridinecarboxamide
CAS No.:1429513-50-7
Molecular Formula:C₂₃H₁₄BrClF₇N₃O₃
Molecular Weight:628.728
Hs Code.:

Synonyms:N-[3-[[[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-(heptafluoro)propyl)phenyl]amino]carbonyl]-2-methoxyphenyl]-4-pyridinecarboxamide

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Chemical Property of N-[3-[[[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-(heptafluoro)propyl)phenyl]amino]carbonyl]-2-methoxyphenyl]-4-pyridinecarboxamide

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Technology Process of N-[3-[[[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-(heptafluoro)propyl)phenyl]amino]carbonyl]-2-methoxyphenyl]-4-pyridinecarboxamide

There total 2 articles about N-[3-[[[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-(heptafluoro)propyl)phenyl]amino]carbonyl]-2-methoxyphenyl]-4-pyridinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1429514-50-0
3-amino-N-[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-heptafluoroprop-2-yl)phenyl]-2-methoxybenzamide

: 39178-35-3
isonicotinoyl chloride hydrochloride

: 1429513-50-7
N-[3-[[[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-(heptafluoro)propyl)phenyl]amino]carbonyl]-2-methoxyphenyl]-4-pyridinecarboxamide

Guidance literature:: With pyridine; In tetrahydrofuran; at 20 ℃; for 26h;

Reference yield:

: 1429514-43-1
N-[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-(heptafluoro)propyl)phenyl]-2-methoxy-3-nitro-benzamide

: 1429513-50-7
N-[3-[[[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-(heptafluoro)propyl)phenyl]amino]carbonyl]-2-methoxyphenyl]-4-pyridinecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammomium bromide; sodium dithionite; sodium hydroxide / tetrahydrofuran / 4 h / Reflux

2: pyridine / tetrahydrofuran / 26 h / 20 °C

With pyridine; sodium dithionite; tetrabutylammomium bromide; sodium hydroxide; In tetrahydrofuran;