1-phenyl-2-(4-chlorobutyl)-C₂B₁₀H₁₀

Base Information

Chemical Name:1-phenyl-2-(4-chlorobutyl)-C₂B₁₀H₁₀
CAS No.:862203-70-1
Molecular Formula:C₁₂H₂₃B₁₀Cl
Molecular Weight:310.878
Hs Code.:

1-phenyl-2-(4-chlorobutyl)-C<sub>2</sub>B<sub>10</sub>H<sub>10</sub>

Synonyms:1-phenyl-2-(4-chlorobutyl)-C₂B₁₀H₁₀

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Chemical Property of 1-phenyl-2-(4-chlorobutyl)-C₂B₁₀H₁₀

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Technology Process of 1-phenyl-2-(4-chlorobutyl)-C₂B₁₀H₁₀

There total 1 articles about 1-phenyl-2-(4-chlorobutyl)-C₂B₁₀H₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10297-05-9
1-chloro 4-iodobutane

: 16390-61-7
1-phenyl-1,2-closo-C₂B₁₀H₁₁

: 862203-70-1
1-phenyl-2-(4-chlorobutyl)-C₂B₁₀H₁₀

: 862203-75-6
1-phenyl-2-(4-iodobutyl)-C₂B₁₀H₁₀

Guidance literature:: With n-butyllithium; In diethyl ether; hexane; benzene; under Ar, Schlenk techniques; B-compd. dissolved in Et2O/benzene (v/v=2/1), cooled to -78°C, n-BuLi in C6H12 added, stored at -78°C for 30 min, warmed to room temp., stirred for 4 h, cooled to 0°C, I-compd. added, stirred for 30 min; H2O added, organic phase separated, aqueous layer extracted with Et2O, solv. removed, thin-layer chromy. (SiO2, n-pentane/ethyl acetate v/v=6/1), elem. anal.;
DOI:10.1021/ja0517116

Reference yield: 95.0%

: 862203-70-1
1-phenyl-2-(4-chlorobutyl)-C₂B₁₀H₁₀

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

: 862203-75-6
1-phenyl-2-(4-iodobutyl)-C₂B₁₀H₁₀

Guidance literature:: In acetone; under Ar, Schlenk technique; mixed, refluxed for 3 days, cooled to room temp., solv removed; extracted with Et2O, extract dried in vac., flash column chromy. (SiO2, n-pentane/ethyl acetate v/v=5/1), elem. anal.;
DOI:10.1021/ja0517116