2-(tert-butoxycarbonyl(3,4-dichlorobenzyl)amino)-1-phenylethyl 3-nitrobenzenesulfonate

Base Information

Chemical Name:2-(tert-butoxycarbonyl(3,4-dichlorobenzyl)amino)-1-phenylethyl 3-nitrobenzenesulfonate
CAS No.:1345986-07-3
Molecular Formula:C₂₆H₂₆Cl₂N₂O₇S
Molecular Weight:581.474
Hs Code.:

Synonyms:2-(tert-butoxycarbonyl(3,4-dichlorobenzyl)amino)-1-phenylethyl 3-nitrobenzenesulfonate

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Chemical Property of 2-(tert-butoxycarbonyl(3,4-dichlorobenzyl)amino)-1-phenylethyl 3-nitrobenzenesulfonate

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Technology Process of 2-(tert-butoxycarbonyl(3,4-dichlorobenzyl)amino)-1-phenylethyl 3-nitrobenzenesulfonate

There total 9 articles about 2-(tert-butoxycarbonyl(3,4-dichlorobenzyl)amino)-1-phenylethyl 3-nitrobenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1345986-15-3
C₂₀H₂₃Cl₂NO₃

: 121-51-7
3-nitrobenzenesulphonyl chloride

: 1345986-07-3
2-(tert-butoxycarbonyl(3,4-dichlorobenzyl)amino)-1-phenylethyl 3-nitrobenzenesulfonate

Guidance literature:: C₂₀H₂₃Cl₂NO₃; With potassium hydroxide; In tetrahydrofuran; for 0.25h;

3-nitrobenzenesulphonyl chloride; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2011.08.078

Reference yield:

: 96-09-3
styrene oxide

: 1345986-07-3
2-(tert-butoxycarbonyl(3,4-dichlorobenzyl)amino)-1-phenylethyl 3-nitrobenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: activated silica / 24 h / Inert atmosphere

2: triethylamine / methanol / 0.5 h / Reflux

3: potassium hydroxide / tetrahydrofuran / 0.25 h

With triethylamine; potassium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2011.08.078

Reference yield:

: 774553-35-4
C₁₅H₁₅Cl₂NO

: 1345986-07-3
2-(tert-butoxycarbonyl(3,4-dichlorobenzyl)amino)-1-phenylethyl 3-nitrobenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / methanol / 0.5 h / Reflux

2: potassium hydroxide / tetrahydrofuran / 0.25 h

With triethylamine; potassium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2011.08.078