3-[5-bromo-1-(tert-butyloxycarbonyl)-1H-indol-3-yl]-4-(1H-pyrrol-2-yl)-1-phenyl-1H-pyrrole-2,5-dione

Base Information

• Chemical Name: 3-[5-bromo-1-(tert-butyloxycarbonyl)-1H-indol-3-yl]-4-(1H-pyrrol-2-yl)-1-phenyl-1H-pyrrole-2,5-dione
• CAS No.: 959418-09-8
• Molecular Formula: C₂₇H₂₂BrN₃O₄
• Molecular Weight: 532.393

Synonyms:3-[5-bromo-1-(tert-butyloxycarbonyl)-1H-indol-3-yl]-4-(1H-pyrrol-2-yl)-1-phenyl-1H-pyrrole-2,5-dione

Chemical Property of 3-[5-bromo-1-(tert-butyloxycarbonyl)-1H-indol-3-yl]-4-(1H-pyrrol-2-yl)-1-phenyl-1H-pyrrole-2,5-dione

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Technology Process of 3-[5-bromo-1-(tert-butyloxycarbonyl)-1H-indol-3-yl]-4-(1H-pyrrol-2-yl)-1-phenyl-1H-pyrrole-2,5-dione

There total 1 articles about 3-[5-bromo-1-(tert-butyloxycarbonyl)-1H-indol-3-yl]-4-(1H-pyrrol-2-yl)-1-phenyl-1H-pyrrole-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

4-chloro-3-[5-bromo-1-(tert-butyloxycarbonyl)-1H-indol-3-yl]-1-phenyl-1H-pyrrole-2,5-dione + pyrrole (109-97-7,30604-81-0) → 3-[5-bromo-1-(tert-butyloxycarbonyl)-1H-indol-3-yl]-4-(1H-pyrrol-2-yl)-1-phenyl-1H-pyrrole-2,5-dione (959418-09-8)

Guidance literature:

pyrrole; With lithium hexamethyldisilazane; In tetrahydrofuran; at -20 ℃; for 1h;

4-chloro-3-[5-bromo-1-(tert-butyloxycarbonyl)-1H-indol-3-yl]-1-phenyl-1H-pyrrole-2,5-dione; In tetrahydrofuran; at 0 ℃; Further stages.;

DOI:10.1248/cpb.55.1302

Reference yield: 48.0%

3-[5-bromo-1-(tert-butyloxycarbonyl)-1H-indol-3-yl]-4-(1H-pyrrol-2-yl)-1-phenyl-1H-pyrrole-2,5-dione (959418-09-8) → C16H10BrN3O2 + C22H14BrN3O2

Guidance literature:

With ammonium acetate; at 150 ℃; for 1h;

DOI:10.1248/cpb.55.1302

upstream raw materials:

pyrrole

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