(S)-2-amino-N-((1Z,6Z)-4-((tert-butyldiphenylsilyl)ox-y)octa-1,6-dien-1-yl)-3,3-dimethylbutanamide

Base Information

Chemical Name:(S)-2-amino-N-((1Z,6Z)-4-((tert-butyldiphenylsilyl)ox-y)octa-1,6-dien-1-yl)-3,3-dimethylbutanamide
CAS No.:960211-45-4
Molecular Formula:C₃₀H₄₄N₂O₂Si
Molecular Weight:492.777
Hs Code.:

Synonyms:(S)-2-amino-N-((1Z,6Z)-4-((tert-butyldiphenylsilyl)ox-y)octa-1,6-dien-1-yl)-3,3-dimethylbutanamide

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Chemical Property of (S)-2-amino-N-((1Z,6Z)-4-((tert-butyldiphenylsilyl)ox-y)octa-1,6-dien-1-yl)-3,3-dimethylbutanamide

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Technology Process of (S)-2-amino-N-((1Z,6Z)-4-((tert-butyldiphenylsilyl)ox-y)octa-1,6-dien-1-yl)-3,3-dimethylbutanamide

There total 9 articles about (S)-2-amino-N-((1Z,6Z)-4-((tert-butyldiphenylsilyl)ox-y)octa-1,6-dien-1-yl)-3,3-dimethylbutanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 960211-42-1
tert-butyl ((S)-1-(((S,1Z,6Z)-4-((tert-butyldiphenylsilyl)oxy)octa-1,6-dien-1-yl)amino)-3,3-dimethyl-1-oxobutan-2-yl)carbamate

: 960211-45-4
(S)-2-amino-N-((1Z,6Z)-4-((tert-butyldiphenylsilyl)ox-y)octa-1,6-dien-1-yl)-3,3-dimethylbutanamide

Guidance literature:: In ethylene glycol; at 200 ℃; for 0.25h;
DOI:10.1016/j.tet.2021.131953

Reference yield:

: 960211-38-5
(S,Z)-3-((tert-butyldiphenylsilyl)oxy)hept-5-enal

: 960211-45-4
(S)-2-amino-N-((1Z,6Z)-4-((tert-butyldiphenylsilyl)ox-y)octa-1,6-dien-1-yl)-3,3-dimethylbutanamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.03 h / 20 °C

1.2: 1.58 h / -78 - 20 °C

2.1: potassium carbonate / copper(l) iodide; N,N`-dimethylethylenediamine / N,N-dimethyl-formamide / 16 - 18 h / 90 °C

3.1: ethylene glycol / 0.17 - 0.33 h / 200 °C

With sodium hexamethyldisilazane; potassium carbonate; ethylene glycol; copper(l) iodide; N,N`-dimethylethylenediamine; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 960211-36-3
(S,Z)-5-(but-2-en-1-yl)-2,2,9,9,10,10-hexamethyl-3,3-diphenyl-4,8-dioxa-3,9-disilaundecane

: 960211-45-4
(S)-2-amino-N-((1Z,6Z)-4-((tert-butyldiphenylsilyl)ox-y)octa-1,6-dien-1-yl)-3,3-dimethylbutanamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: ethanol / pyridinium p-toluenesulfonate / 7 h / 20 °C

2.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 16 - 18 h / 20 °C

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.03 h / 20 °C

3.2: 1.58 h / -78 - 20 °C

4.1: potassium carbonate / copper(l) iodide; N,N`-dimethylethylenediamine / N,N-dimethyl-formamide / 16 - 18 h / 90 °C

5.1: ethylene glycol / 0.17 - 0.33 h / 200 °C

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; ethanol; [bis(acetoxy)iodo]benzene; sodium hexamethyldisilazane; potassium carbonate; ethylene glycol; copper(l) iodide; pyridinium p-toluenesulfonate; N,N`-dimethylethylenediamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;