(1S,2S)-1,2-bis(2-methoxyphenyl)-N,N'-bis[(S)-1-phenylethyl]-1,2-ethanediamine

Base Information

Chemical Name:(1S,2S)-1,2-bis(2-methoxyphenyl)-N,N'-bis[(S)-1-phenylethyl]-1,2-ethanediamine
CAS No.:693225-14-8
Molecular Formula:C₃₂H₃₆N₂O₂
Molecular Weight:480.65
Hs Code.:

Synonyms:(1S,2S)-1,2-bis(2-methoxyphenyl)-N,N'-bis[(S)-1-phenylethyl]-1,2-ethanediamine

Suppliers and Price of (1S,2S)-1,2-bis(2-methoxyphenyl)-N,N'-bis[(S)-1-phenylethyl]-1,2-ethanediamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1S,2S)-1,2-bis(2-methoxyphenyl)-N,N'-bis[(S)-1-phenylethyl]-1,2-ethanediamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1S,2S)-1,2-bis(2-methoxyphenyl)-N,N'-bis[(S)-1-phenylethyl]-1,2-ethanediamine

There total 1 articles about (1S,2S)-1,2-bis(2-methoxyphenyl)-N,N'-bis[(S)-1-phenylethyl]-1,2-ethanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 578-57-4
2-bromoanisole

: 138812-17-6
N,N'-bis<(S)-1-phenylethyl>ethanediimine

: 758691-47-3
(1R,2R)-1,2-bis(2-methoxyphenyl)-N,N'-bis[(S)-1-phenylethyl]-1,2-ethanediamine

: 693225-14-8
(1S,2S)-1,2-bis(2-methoxyphenyl)-N,N'-bis[(S)-1-phenylethyl]-1,2-ethanediamine

Guidance literature:: 2-bromoanisole; With iodine; magnesium; In tetrahydrofuran; at 60 ℃; for 1h;

N,N'-bis<(S)-1-phenylethyl>ethanediimine; In tetrahydrofuran; at 0 - 25 ℃; for 2h; Further stages.;
DOI:10.1002/ejoc.200400129

Reference yield: 75.0%

: 693225-14-8
(1S,2S)-1,2-bis(2-methoxyphenyl)-N,N'-bis[(S)-1-phenylethyl]-1,2-ethanediamine

: 148240-65-7
(1S,2S)-1,2-bis(2-methoxyphenyl)-1,2-ethanediamine

Guidance literature:: With ammonium formate; palladium on activated charcoal; In methanol; for 10h; Heating;
DOI:10.1002/ejoc.200400129

Reference yield:

: 693225-14-8
(1S,2S)-1,2-bis(2-methoxyphenyl)-N,N'-bis[(S)-1-phenylethyl]-1,2-ethanediamine

: (1S,2S)-N,N'-dibenzyl-1,2-bis(2-methoxyphenyl)-1,2-ethanediamine

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / HCO₂NH₄ / Pd/C / methanol / 10 h / Heating

2: 58 percent / triethylamine; 4-(dimethylamino)pyridine / CH₂Cl₂ / 0 - 25 °C

3: 49 percent / BH₃-SMe₂ / tetrahydrofuran / 6 h / Heating

With dmap; dimethylsulfide borane complex; ammonium formate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/ejoc.200400129