(5S,10S)-5,10-dibenzyl-3,12-dioxa-6,9,18-triazabicyclo[12.3.1]octadeca-1⁽¹⁸⁾,14,16-triene-2,7,8,13-tetraone

Base Information

• Chemical Name: (5S,10S)-5,10-dibenzyl-3,12-dioxa-6,9,18-triazabicyclo[12.3.1]octadeca-1⁽¹⁸⁾,14,16-triene-2,7,8,13-tetraone
• CAS No.: 1597413-15-4
• Molecular Formula: C₂₇H₂₅N₃O₆
• Molecular Weight: 487.512

Synonyms:(5S,10S)-5,10-dibenzyl-3,12-dioxa-6,9,18-triazabicyclo[12.3.1]octadeca-1⁽¹⁸⁾,14,16-triene-2,7,8,13-tetraone

Chemical Property of (5S,10S)-5,10-dibenzyl-3,12-dioxa-6,9,18-triazabicyclo[12.3.1]octadeca-1⁽¹⁸⁾,14,16-triene-2,7,8,13-tetraone

Chemical Property:

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Technology Process of (5S,10S)-5,10-dibenzyl-3,12-dioxa-6,9,18-triazabicyclo[12.3.1]octadeca-1⁽¹⁸⁾,14,16-triene-2,7,8,13-tetraone

There total 1 articles about (5S,10S)-5,10-dibenzyl-3,12-dioxa-6,9,18-triazabicyclo[12.3.1]octadeca-1⁽¹⁸⁾,14,16-triene-2,7,8,13-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

2,6-Pyridinedicarbonyl dichloride (3739-94-4) + (S)-N,N'-bis<1-(hydroxymethyl)-2-phenylethyl>ethanediamide (19071-60-4,133464-01-4) → (5S,10S)-5,10-dibenzyl-3,12-dioxa-6,9,18-triazabicyclo[12.3.1]octadeca-1(18),14,16-triene-2,7,8,13-tetraone (1597413-15-4)

Guidance literature:

With triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; benzene; for 120h; Reflux;

DOI:10.1016/j.tetasy.2014.01.009

Reference yield:

(5S,10S)-5,10-dibenzyl-3,12-dioxa-6,9,18-triazabicyclo[12.3.1]octadeca-1(18),14,16-triene-2,7,8,13-tetraone (1597413-15-4) + (S)-α-(1-naphthyl)ethylammonium perchlorate (82431-48-9) → C12H13N*ClHO4*C27H25N3O6

Guidance literature:

In dimethylsulfoxide-d6; at 25 ℃;

DOI:10.1016/j.tetasy.2014.01.009

Reference yield:

(5S,10S)-5,10-dibenzyl-3,12-dioxa-6,9,18-triazabicyclo[12.3.1]octadeca-1(18),14,16-triene-2,7,8,13-tetraone (1597413-15-4) + (R)-α-phenylethylamine hydrogen perchlorate (69128-54-7,73351-60-7,73395-23-0) → C8H11N*ClHO4*C27H25N3O6 (1597413-22-3)

Guidance literature:

In dimethylsulfoxide-d6; at 25 ℃;

DOI:10.1016/j.tetasy.2014.01.009

upstream raw materials:

2,6-Pyridinedicarbonyl dichloride

(S)-N,N'-bis<1-(hydroxymethyl)-2-phenylethyl>ethanediamide

Downstream raw materials:

C₈H₁₁N*ClHO₄*C₂₇H₂₅N₃O₆

C₈H₁₁N*ClHO₄*C₂₇H₂₅N₃O₆

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