C₂₂H₃₀O₆Si

Base Information

Chemical Name:C₂₂H₃₀O₆Si
CAS No.:1361049-61-7
Molecular Formula:C₂₂H₃₀O₆Si
Molecular Weight:418.562
Hs Code.:

C<sub>22</sub>H<sub>30</sub>O<sub>6</sub>Si

Synonyms:C₂₂H₃₀O₆Si

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Chemical Property of C₂₂H₃₀O₆Si

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Technology Process of C₂₂H₃₀O₆Si

There total 8 articles about C₂₂H₃₀O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1361049-72-0
(5R,2'R)-3-(benzyloxy)-5-[2'-(tert-butyldimethylsilyloxy)but-3'-enyl]-4-(methoxycarbonyl)furan-2(5H)-one

: 1361049-61-7
C₂₂H₃₀O₆Si

Guidance literature:: With barium hydroxide octahydrate; In tetrahydrofuran; water; at 20 ℃; for 60h;
DOI:10.1002/anie.201106889

Reference yield:

: 1361049-70-8
methyl (5R)-5-hydroxy-3-oxo-6-heptenoate

: 1361049-61-7
C₂₂H₃₀O₆Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetic acid; tetramethylammonium triacetoxyborohydride / acetonitrile / 44 h / -35 °C

2.1: 2,6-dimethylpyridine / dichloromethane / 4 h / -78 °C

3.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 1 h / -78 °C

3.2: 19 h / -78 - 20 °C

3.3: 21 h / -78 - 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C

4.2: 21 h / 20 °C

5.1: barium hydroxide octahydrate / tetrahydrofuran; water / 60 h / 20 °C

With 2,6-dimethylpyridine; barium hydroxide octahydrate; sodium hydride; acetic acid; tetramethylammonium triacetoxyborohydride; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1002/anie.201106889

Reference yield:

: 521315-88-8
methyl (3R,5R)-3,5-dihydroxy-6-heptenoate

: 1361049-61-7
C₂₂H₃₀O₆Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 4 h / -78 °C

2.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: 19 h / -78 - 20 °C

2.3: 21 h / -78 - 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C

3.2: 21 h / 20 °C

4.1: barium hydroxide octahydrate / tetrahydrofuran; water / 60 h / 20 °C

With 2,6-dimethylpyridine; barium hydroxide octahydrate; sodium hydride; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/anie.201106889