[(3-Methylisoxazol-5-YL)methyl]triphenylphosphonium chloride

Base Information

Chemical Name:[(3-Methylisoxazol-5-YL)methyl]triphenylphosphonium chloride
CAS No.:75624-75-8
Molecular Formula:C23H21 N O P . Cl
Molecular Weight:393.853
Hs Code.:
European Community (EC) Number:278-268-5
DSSTox Substance ID:DTXSID80997060
Mol file:75624-75-8.mol

Synonyms:75624-75-8;EINECS 278-268-5;[(3-METHYLISOXAZOL-5-YL)METHYL]TRIPHENYLPHOSPHONIUM CHLORIDE;((3-Methylisoxazol-5-yl)methyl)triphenylphosphonium chloride;C23H21NOP.Cl;SCHEMBL10891834;C23-H21-N-O-P.Cl;DTXSID80997060;[(3-Methyl-1,2-oxazol-5-yl)methyl](triphenyl)phosphanium chloride

Suppliers and Price of [(3-Methylisoxazol-5-YL)methyl]triphenylphosphonium chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of [(3-Methylisoxazol-5-YL)methyl]triphenylphosphonium chloride

Chemical Property:

PSA：39.62000
LogP:1.48110
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:393.1049290
Heavy Atom Count:27
Complexity:378

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NOC(=C1)C[P+](C2=CC=CC=C2)(C3=CC=CC=C3)C4=CC=CC=C4.[Cl-]

Technology Process of [(3-Methylisoxazol-5-YL)methyl]triphenylphosphonium chloride

There total 4 articles about [(3-Methylisoxazol-5-YL)methyl]triphenylphosphonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 75624-67-8
(2,4-Dioxopentyl)triphenylphosphonium-chlorid

: 75624-75-8
(3-Methyl-5-isoxazolylmethyl)triphenylphosphonium-chlorid

Guidance literature:: With hydroxylamine hydrochloride; In water; 1.) room temp., 16 h, 2.) reflux, 4 h;

Reference yield:

: 75624-65-6
4-Methoxy-5-(triphenylphosphoranyliden)-3-penten-2-on

: 75624-75-8
(3-Methyl-5-isoxazolylmethyl)triphenylphosphonium-chlorid

Guidance literature:: Multi-step reaction with 2 steps

1: 1 N HCl / 3 h / Heating

2: 71 percent / NH₂OH*HCl / H₂O / 1.) room temp., 16 h, 2.) reflux, 4 h

With hydrogenchloride; hydroxylamine hydrochloride; In water;

Reference yield:

: 60661-64-5
(2-Methoxy-1-propenyl)triphenylphosphonium-bromid

: 75624-75-8
(3-Methyl-5-isoxazolylmethyl)triphenylphosphonium-chlorid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi / 1.) THF, hexane, -30 deg C, 90 min, 2.) THF, -30 deg C, 2 h

2: 1 N HCl / 3 h / Heating

3: 71 percent / NH₂OH*HCl / H₂O / 1.) room temp., 16 h, 2.) reflux, 4 h

With hydrogenchloride; n-butyllithium; hydroxylamine hydrochloride; In water;