3-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecane-1-sulfonyl)-3-(2-nitrobenzyl)-1-propyl-5-p-tolyl-1,3-dihydroindol-2-one

Base Information

• Chemical Name: 3-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecane-1-sulfonyl)-3-(2-nitrobenzyl)-1-propyl-5-p-tolyl-1,3-dihydroindol-2-one
• CAS No.: 1007402-24-5
• Molecular Formula: C₃₅H₂₇F₁₇N₂O₅S
• Molecular Weight: 910.649

Synonyms:3-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecane-1-sulfonyl)-3-(2-nitrobenzyl)-1-propyl-5-p-tolyl-1,3-dihydroindol-2-one

Chemical Property of 3-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecane-1-sulfonyl)-3-(2-nitrobenzyl)-1-propyl-5-p-tolyl-1,3-dihydroindol-2-one

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Technology Process of 3-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecane-1-sulfonyl)-3-(2-nitrobenzyl)-1-propyl-5-p-tolyl-1,3-dihydroindol-2-one

There total 1 articles about 3-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecane-1-sulfonyl)-3-(2-nitrobenzyl)-1-propyl-5-p-tolyl-1,3-dihydroindol-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

5-bromo-3-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecane-1-sulfonyl)-3-(2-nitrobenzyl)-1-propyl-1,3-dihydroindol-2-one (1007402-19-8) + 4-methylphenylboronic acid (5720-05-8) → 3-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecane-1-sulfonyl)-3-(2-nitrobenzyl)-1-propyl-5-p-tolyl-1,3-dihydroindol-2-one (1007402-24-5)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,4-dioxane; water; at 80 ℃; for 19h;

DOI:10.1021/ol800070y

Reference yield: 51.0%

3-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecane-1-sulfonyl)-3-(2-nitrobenzyl)-1-propyl-5-p-tolyl-1,3-dihydroindol-2-one (1007402-24-5) → 3-(2-aminobenzyl)-1-propyl-5-p-tolyl-1,3-dihydroindol-2-one (1007402-27-8)

Guidance literature:

With samarium diiodide; In tetrahydrofuran; at 20 ℃; for 48h; Inert atmosphere;

DOI:10.1021/ol800070y

Reference yield: 30.0%

3-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecane-1-sulfonyl)-3-(2-nitrobenzyl)-1-propyl-5-p-tolyl-1,3-dihydroindol-2-one (1007402-24-5) → C25H24N2O (1007402-33-6) + 3-(2-aminobenzyl)-3-hydroxy-1-propyl-5-p-tolyl-1,3-dihydroindol-2-one (1007402-34-7)

Guidance literature:

With samarium diiodide; In tetrahydrofuran; at 20 ℃; for 3.5h; Inert atmosphere;

DOI:10.1021/ol800070y

upstream raw materials:

5-bromo-3-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecane-1-sulfonyl)-3-(2-nitrobenzyl)-1-propyl-1,3-dihydroindol-2-one

4-methylphenylboronic acid

Downstream raw materials:

3-(2-aminobenzyl)-1-propyl-5-p-tolyl-1,3-dihydroindol-2-one

C₂₅H₂₄N₂O

3-(2-aminobenzyl)-3-hydroxy-1-propyl-5-p-tolyl-1,3-dihydroindol-2-one

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