(S)-pent-4-en-2-yl 3-allyl-6-((E)-4-((4S,5R)-2,2-dimethyl-5-((Z)-prop-1-enyl)-1,3-diox-olan-4-yl)but-1-enyl)-2,4-dihydroxybenzoate

Base Information

• Chemical Name: (S)-pent-4-en-2-yl 3-allyl-6-((E)-4-((4S,5R)-2,2-dimethyl-5-((Z)-prop-1-enyl)-1,3-diox-olan-4-yl)but-1-enyl)-2,4-dihydroxybenzoate
• CAS No.: 1334484-95-5
• Molecular Formula: C₂₇H₃₆O₆
• Molecular Weight: 456.579

Synonyms:(S)-pent-4-en-2-yl 3-allyl-6-((E)-4-((4S,5R)-2,2-dimethyl-5-((Z)-prop-1-enyl)-1,3-diox-olan-4-yl)but-1-enyl)-2,4-dihydroxybenzoate

Chemical Property of (S)-pent-4-en-2-yl 3-allyl-6-((E)-4-((4S,5R)-2,2-dimethyl-5-((Z)-prop-1-enyl)-1,3-diox-olan-4-yl)but-1-enyl)-2,4-dihydroxybenzoate

Chemical Property:

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Technology Process of (S)-pent-4-en-2-yl 3-allyl-6-((E)-4-((4S,5R)-2,2-dimethyl-5-((Z)-prop-1-enyl)-1,3-diox-olan-4-yl)but-1-enyl)-2,4-dihydroxybenzoate

There total 3 articles about (S)-pent-4-en-2-yl 3-allyl-6-((E)-4-((4S,5R)-2,2-dimethyl-5-((Z)-prop-1-enyl)-1,3-diox-olan-4-yl)but-1-enyl)-2,4-dihydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C27H38O7 → (S)-pent-4-en-2-yl 3-allyl-6-((E)-4-((4S,5R)-2,2-dimethyl-5-((Z)-prop-1-enyl)-1,3-diox-olan-4-yl)but-1-enyl)-2,4-dihydroxybenzoate (1334484-95-5)

Guidance literature:

C₂₇H₃₈O₇; With cesium acetate; In dichloromethane; isopropyl alcohol; at 25 ℃; for 3h; Inert atmosphere;

With acetic acid; In dichloromethane; isopropyl alcohol; for 18h; Inert atmosphere;

DOI:10.1021/ol202320m

Reference yield:

C26H34O9 (1334484-90-0) → (S)-pent-4-en-2-yl 3-allyl-6-((E)-4-((4S,5R)-2,2-dimethyl-5-((Z)-prop-1-enyl)-1,3-diox-olan-4-yl)but-1-enyl)-2,4-dihydroxybenzoate (1334484-95-5)

Guidance literature:

Multi-step reaction with 3 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.1: toluene / 1 h / Reflux; Inert atmosphere

3.1: cesium acetate / dichloromethane; isopropyl alcohol / 3 h / 25 °C / Inert atmosphere

3.2: 18 h / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; cesium acetate; In dichloromethane; isopropyl alcohol; toluene;

DOI:10.1021/ol202320m

Reference yield:

C25H34O7 → (S)-pent-4-en-2-yl 3-allyl-6-((E)-4-((4S,5R)-2,2-dimethyl-5-((Z)-prop-1-enyl)-1,3-diox-olan-4-yl)but-1-enyl)-2,4-dihydroxybenzoate (1334484-95-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: toluene / 1 h / Reflux; Inert atmosphere

2.1: cesium acetate / dichloromethane; isopropyl alcohol / 3 h / 25 °C / Inert atmosphere

2.2: 18 h / Inert atmosphere

With cesium acetate; In dichloromethane; isopropyl alcohol; toluene;

DOI:10.1021/ol202320m

upstream raw materials:

C₂₆H₃₄O₉

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