C₁₄H₁₉BrO₂

Base Information

Chemical Name:C₁₄H₁₉BrO₂
CAS No.:1389321-64-5
Molecular Formula:C₁₄H₁₉BrO₂
Molecular Weight:299.208
Hs Code.:

C<sub>14</sub>H<sub>19</sub>BrO<sub>2</sub>

Synonyms:C₁₄H₁₉BrO₂

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Chemical Property of C₁₄H₁₉BrO₂

Chemical Property:

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Technology Process of C₁₄H₁₉BrO₂

There total 8 articles about C₁₄H₁₉BrO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1389321-63-4
C₂₀H₃₃BrO₂Si

: 1389321-64-5
C₁₄H₁₉BrO₂

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1055/s-0031-1291047

Reference yield:

: C₉H₈Br₂O₂

: 1389321-64-5
C₁₄H₁₉BrO₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: boron trifluoride diethyl etherate / tetrahydrofuran / 1 h / 20 °C

2.1: titanium tetrachloride / dichloromethane / 0.17 h / 0 °C

2.2: 0.5 h / 0 °C

2.3: 3.5 h / -78 - 0 °C

3.1: 1H-imidazole / dichloromethane / 24 h / 20 °C

4.1: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 20 °C

5.1: tetrahydrofuran / 0 °C

6.1: n-butyllithium / tetrahydrofuran; hexane / 0.58 h / 0 - 20 °C

6.2: 0 - 20 °C

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 24 h / 20 °C

With 1H-imidazole; n-butyllithium; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; titanium tetrachloride; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; 2.3: Evans syn aldol reaction / 6.2: Wittig reaction;
DOI:10.1055/s-0031-1291047

Reference yield:

: 1183778-97-3
2-bromo-1-(2-bromo-4-methoxyphenyl)ethan-1-one

: 1389321-64-5
C₁₄H₁₉BrO₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C

1.2: 3 h / 20 °C

2.1: boron trifluoride diethyl etherate / tetrahydrofuran / 1 h / 20 °C

3.1: titanium tetrachloride / dichloromethane / 0.17 h / 0 °C

3.2: 0.5 h / 0 °C

3.3: 3.5 h / -78 - 0 °C

4.1: 1H-imidazole / dichloromethane / 24 h / 20 °C

5.1: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 20 °C

6.1: tetrahydrofuran / 0 °C

7.1: n-butyllithium / tetrahydrofuran; hexane / 0.58 h / 0 - 20 °C

7.2: 0 - 20 °C

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 24 h / 20 °C

With 1H-imidazole; sodium tetrahydroborate; n-butyllithium; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; titanium tetrachloride; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; 3.3: Evans syn aldol reaction / 7.2: Wittig reaction;
DOI:10.1055/s-0031-1291047