2-Isopropoxy-4-methoxy-N-(1H-tetrazol-5-yl)-3-trimethylsilanyl-benzamide

Base Information

Chemical Name:2-Isopropoxy-4-methoxy-N-(1H-tetrazol-5-yl)-3-trimethylsilanyl-benzamide
CAS No.:117401-92-0
Molecular Formula:C₁₅H₂₃N₅O₃Si
Molecular Weight:349.465
Hs Code.:

Synonyms:2-Isopropoxy-4-methoxy-N-(1H-tetrazol-5-yl)-3-trimethylsilanyl-benzamide

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Chemical Property of 2-Isopropoxy-4-methoxy-N-(1H-tetrazol-5-yl)-3-trimethylsilanyl-benzamide

Chemical Property:

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Technology Process of 2-Isopropoxy-4-methoxy-N-(1H-tetrazol-5-yl)-3-trimethylsilanyl-benzamide

There total 4 articles about 2-Isopropoxy-4-methoxy-N-(1H-tetrazol-5-yl)-3-trimethylsilanyl-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5446-02-6
4-methoxymethylsalicylate

: 117401-92-0
2-Isopropoxy-4-methoxy-N-(1H-tetrazol-5-yl)-3-trimethylsilanyl-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 61 percent / potassium tert-butoxide / dimethylsulfoxide / 20 h / Ambient temperature

2: 60 percent / lithium diisopropylamide / tetrahydrofuran; hexane / 20 h / -70 - 20 °C

3: 89 percent / 1.0 N aq. NaOH / methanol; tetrahydrofuran / 6 h / Heating

4: 1.) 1,1'-carbonyldiimidazole (CDI), 2.) triethylamine / 1.) acetonitrile, reflux, 30 min, 2.) acetonitrile, reflux, 18 h

With sodium hydroxide; potassium tert-butylate; triethylamine; 1,1'-carbonyldiimidazole; lithium diisopropyl amide; In tetrahydrofuran; methanol; hexane; dimethyl sulfoxide;
DOI:10.1021/jm00111a039

Reference yield:

: 117401-87-3
methyl 4-methoxy-2-(1-methylethoxy)benzoate

: 117401-92-0
2-Isopropoxy-4-methoxy-N-(1H-tetrazol-5-yl)-3-trimethylsilanyl-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / lithium diisopropylamide / tetrahydrofuran; hexane / 20 h / -70 - 20 °C

2: 89 percent / 1.0 N aq. NaOH / methanol; tetrahydrofuran / 6 h / Heating

3: 1.) 1,1'-carbonyldiimidazole (CDI), 2.) triethylamine / 1.) acetonitrile, reflux, 30 min, 2.) acetonitrile, reflux, 18 h

With sodium hydroxide; triethylamine; 1,1'-carbonyldiimidazole; lithium diisopropyl amide; In tetrahydrofuran; methanol; hexane;
DOI:10.1021/jm00111a039

Reference yield:

: 117401-88-4
methyl 4-methoxy-2-(1-methylethoxy)-3-(trimethylsilyl)benzoate

: 117401-92-0
2-Isopropoxy-4-methoxy-N-(1H-tetrazol-5-yl)-3-trimethylsilanyl-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / 1.0 N aq. NaOH / methanol; tetrahydrofuran / 6 h / Heating

2: 1.) 1,1'-carbonyldiimidazole (CDI), 2.) triethylamine / 1.) acetonitrile, reflux, 30 min, 2.) acetonitrile, reflux, 18 h

With sodium hydroxide; triethylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran; methanol;
DOI:10.1021/jm00111a039