C₃₆H₂₈ClNO₇

Base Information

Chemical Name:C₃₆H₂₈ClNO₇
CAS No.:1314420-15-9
Molecular Formula:C₃₆H₂₈ClNO₇
Molecular Weight:622.074
Hs Code.:

C<sub>36</sub>H<sub>28</sub>ClNO<sub>7</sub>

Synonyms:C₃₆H₂₈ClNO₇

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Chemical Property of C₃₆H₂₈ClNO₇

Chemical Property:

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Technology Process of C₃₆H₂₈ClNO₇

There total 5 articles about C₃₆H₂₈ClNO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1314420-13-7
C₃₆H₃₀ClNO₆

: 1314420-15-9
C₃₆H₂₈ClNO₇

Guidance literature:: With selenium(IV) oxide; In 1,4-dioxane; at 135 ℃; for 36h; Inert atmosphere;
DOI:10.1002/anie.201101621

Reference yield:

: 1314420-11-5
C₃₇H₃₄ClNO₇

: 1314420-15-9
C₃₆H₂₈ClNO₇

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / nitromethane / 0 - 20 °C / Inert atmosphere

2: selenium(IV) oxide / 1,4-dioxane / 36 h / 135 °C / Inert atmosphere

With selenium(IV) oxide; boron trifluoride diethyl etherate; In 1,4-dioxane; nitromethane;
DOI:10.1002/anie.201101621

Reference yield:

: 885592-69-8
(2S,4R,5R)-4-(benzyloxy)-5-((benzyloxy)methyl)-2-methoxydihydrofuran-3(2H)-one

: 1314420-15-9
C₃₆H₂₈ClNO₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.17 h / -78 °C / Inert atmosphere

2.1: dmap; triethylamine / dichloromethane / 24 h / 20 °C / Inert atmosphere

3.1: boron trifluoride diethyl etherate / nitromethane / 0 - 20 °C / Inert atmosphere

4.1: selenium(IV) oxide / 1,4-dioxane / 36 h / 135 °C / Inert atmosphere

With dmap; selenium(IV) oxide; boron trifluoride diethyl etherate; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; nitromethane; dichloromethane; 1.1: Aldol reaction / 1.2: Aldol reaction;
DOI:10.1002/anie.201101621