(E)-4-benzylidene-3,5-diphenyl-1-(toluene-4-sulfonyl)-4,5-dihydro-1H-pyrazole

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Chemical Name:(E)-4-benzylidene-3,5-diphenyl-1-(toluene-4-sulfonyl)-4,5-dihydro-1H-pyrazole
CAS No.:1643618-05-6
Molecular Formula:C₂₉H₂₄N₂O₂S
Molecular Weight:464.588
Hs Code.:

Synonyms:(E)-4-benzylidene-3,5-diphenyl-1-(toluene-4-sulfonyl)-4,5-dihydro-1H-pyrazole

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Chemical Property of (E)-4-benzylidene-3,5-diphenyl-1-(toluene-4-sulfonyl)-4,5-dihydro-1H-pyrazole

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Technology Process of (E)-4-benzylidene-3,5-diphenyl-1-(toluene-4-sulfonyl)-4,5-dihydro-1H-pyrazole

There total 4 articles about (E)-4-benzylidene-3,5-diphenyl-1-(toluene-4-sulfonyl)-4,5-dihydro-1H-pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1643618-22-7
C₂₉H₂₄N₂O₂S

: 1643618-05-6
(E)-4-benzylidene-3,5-diphenyl-1-(toluene-4-sulfonyl)-4,5-dihydro-1H-pyrazole

Guidance literature:: With iron(III) chloride; In dichloromethane; at 20 ℃; for 0.0833333h; regioselective reaction;
DOI:10.1039/c4ob00550c

Reference yield: 34.0%

: 1643618-22-7
C₂₉H₂₄N₂O₂S

: 1643618-05-6
(E)-4-benzylidene-3,5-diphenyl-1-(toluene-4-sulfonyl)-4,5-dihydro-1H-pyrazole

: 1643617-89-3
3,5-diphenyl-4-[phenyl(toluene-4-sulfonyl)methyl]-1H-pyrazole

Guidance literature:: With iron(III) chloride; at 20 ℃; for 0.0833333h; Reagent/catalyst;
DOI:10.1039/c4ob00550c

Reference yield:

: 1192545-22-4
C₂₉H₂₄N₂O₂S

: 1643618-05-6
(E)-4-benzylidene-3,5-diphenyl-1-(toluene-4-sulfonyl)-4,5-dihydro-1H-pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; triethylamine / tetrahydrofuran / 20 °C

2: iron(III) chloride / dichloromethane / 0.08 h / 20 °C

With iron(III) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c4ob00550c