2-(1-methyl-4-nitro-1H-pyrrole-2-carbonyl)-N-(4-nitrophenyl)hydrazinecarboxamide

Base Information

Chemical Name:2-(1-methyl-4-nitro-1H-pyrrole-2-carbonyl)-N-(4-nitrophenyl)hydrazinecarboxamide
CAS No.:1616260-87-7
Molecular Formula:C₁₃H₁₂N₆O₆
Molecular Weight:348.275
Hs Code.:

Synonyms:2-(1-methyl-4-nitro-1H-pyrrole-2-carbonyl)-N-(4-nitrophenyl)hydrazinecarboxamide

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Chemical Property of 2-(1-methyl-4-nitro-1H-pyrrole-2-carbonyl)-N-(4-nitrophenyl)hydrazinecarboxamide

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Technology Process of 2-(1-methyl-4-nitro-1H-pyrrole-2-carbonyl)-N-(4-nitrophenyl)hydrazinecarboxamide

There total 4 articles about 2-(1-methyl-4-nitro-1H-pyrrole-2-carbonyl)-N-(4-nitrophenyl)hydrazinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 100-28-7
4-Nitrophenyl isocyanate

: 28494-50-0
1-methyl-4-nitropyrrole-2-carboxylic acid hydrazide

: 1616260-87-7
2-(1-methyl-4-nitro-1H-pyrrole-2-carbonyl)-N-(4-nitrophenyl)hydrazinecarboxamide

Guidance literature:: In ethanol; N,N-dimethyl-formamide; Inert atmosphere; Reflux;
DOI:10.1016/j.bmcl.2014.05.018

Reference yield:

: 96-54-8
N-Methylpyrrole

: 1616260-87-7
2-(1-methyl-4-nitro-1H-pyrrole-2-carbonyl)-N-(4-nitrophenyl)hydrazinecarboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / diethyl ether

2: nitric acid; acetic anhydride / 2 h / -10 °C

3: hydrazine hydrate / ethanol / 2 h / 20 °C

4: ethanol; N,N-dimethyl-formamide / Inert atmosphere; Reflux

With nitric acid; acetic anhydride; potassium carbonate; hydrazine hydrate; In diethyl ether; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.05.018

Reference yield:

: 21898-65-7
1-methyl-2-trichloroacetyl-1H-pyrrole

: 1616260-87-7
2-(1-methyl-4-nitro-1H-pyrrole-2-carbonyl)-N-(4-nitrophenyl)hydrazinecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: nitric acid; acetic anhydride / 2 h / -10 °C

2: hydrazine hydrate / ethanol / 2 h / 20 °C

3: ethanol; N,N-dimethyl-formamide / Inert atmosphere; Reflux

With nitric acid; acetic anhydride; hydrazine hydrate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.05.018