(S)-1-(benzyloxycarbonyl)-2-methylpropyl 4-(trans-4-heptylcyclohexyl)benzoate

Base Information

Chemical Name:(S)-1-(benzyloxycarbonyl)-2-methylpropyl 4-(trans-4-heptylcyclohexyl)benzoate
CAS No.:125150-37-0
Molecular Formula:C₃₂H₄₄O₄
Molecular Weight:492.699
Hs Code.:

Synonyms:(S)-1-(benzyloxycarbonyl)-2-methylpropyl 4-(trans-4-heptylcyclohexyl)benzoate

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Chemical Property of (S)-1-(benzyloxycarbonyl)-2-methylpropyl 4-(trans-4-heptylcyclohexyl)benzoate

Chemical Property:

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Technology Process of (S)-1-(benzyloxycarbonyl)-2-methylpropyl 4-(trans-4-heptylcyclohexyl)benzoate

There total 3 articles about (S)-1-(benzyloxycarbonyl)-2-methylpropyl 4-(trans-4-heptylcyclohexyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 65355-31-9
4'-benzoesaeure

: 65138-05-8
(S)-2-hydroxy-3-methylbutyric acid benzyl ester

: 125150-37-0
(S)-1-(benzyloxycarbonyl)-2-methylpropyl 4-(trans-4-heptylcyclohexyl)benzoate

Guidance literature:: With 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; In dichloromethane; for 6h; Ambient temperature;

Reference yield:

: 72-18-4,25609-85-2,7004-03-7,921-10-8
L-valine

: 125150-37-0
(S)-1-(benzyloxycarbonyl)-2-methylpropyl 4-(trans-4-heptylcyclohexyl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaNO₂, 0.5 M H₂SO₄, 2.) NaOH / 1.) water, -2-0 deg C, 3 h, overnight, room temp., 2.) water, pH=4.5-5.0

2: 96 percent / dimethylformamide / 24 h / Ambient temperature

3: 58 percent / DCC, 4-(N-pyrrolidino)pyridine / CH₂Cl₂ / 6 h / Ambient temperature

With sodium hydroxide; sulfuric acid; 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; sodium nitrite; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 54641-19-9
(S)-(-)-sodium 2-hydroxy-3-methylbutanoate

: 125150-37-0
(S)-1-(benzyloxycarbonyl)-2-methylpropyl 4-(trans-4-heptylcyclohexyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / dimethylformamide / 24 h / Ambient temperature

2: 58 percent / DCC, 4-(N-pyrrolidino)pyridine / CH₂Cl₂ / 6 h / Ambient temperature

With 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;