(+/-)-4-Phosphonophenylglycine hydrochloride

Base Information

Chemical Name:(+/-)-4-Phosphonophenylglycine hydrochloride
CAS No.:120667-18-7
Molecular Formula:C₈H₁₀NO₅P*ClH
Molecular Weight:267.606
Hs Code.:

Synonyms:(+/-)-4-Phosphonophenylglycine hydrochloride

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Chemical Property of (+/-)-4-Phosphonophenylglycine hydrochloride

Chemical Property:

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Technology Process of (+/-)-4-Phosphonophenylglycine hydrochloride

There total 3 articles about (+/-)-4-Phosphonophenylglycine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 120667-18-7
(+/-)-4-Phosphonophenylglycine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 0.95 g / methanesulfonic acid / 120 h / Ambient temperature

2: triethylamine / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / toluene / 2.5 h / 105 °C

3: 0.34 g / 6 N aq. HCl / 18 h / Heating

With hydrogenchloride; methanesulfonic acid; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene;
DOI:10.1021/jm00127a030

Reference yield:

: 120667-30-3
α-(benzoylamino)-4-bromobenzeneacetic acid

: 120667-18-7
(+/-)-4-Phosphonophenylglycine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / toluene / 2.5 h / 105 °C

2: 0.34 g / 6 N aq. HCl / 18 h / Heating

With hydrogenchloride; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene;
DOI:10.1021/jm00127a030