2,2'-dithiobismethyl>-1H-indole-3-propanamide>

Base Information

Chemical Name:2,2'-dithiobismethyl>-1H-indole-3-propanamide>
CAS No.:153408-50-5
Molecular Formula:C₄₀H₃₈N₄O₆S₂
Molecular Weight:734.897
Hs Code.:

2,2'-dithiobis<N-<<4-(methoxycarbonyl)phenyl>methyl>-1H-indole-3-propanamide>

Synonyms:2,2'-dithiobismethyl>-1H-indole-3-propanamide>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2'-dithiobismethyl>-1H-indole-3-propanamide>

Chemical Property:

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Technology Process of 2,2'-dithiobismethyl>-1H-indole-3-propanamide>

There total 3 articles about 2,2'-dithiobismethyl>-1H-indole-3-propanamide> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 830-96-6
Indole-3-propionic acid

: 153408-50-5
2,2'-dithiobismethyl>-1H-indole-3-propanamide>

Guidance literature:: Multi-step reaction with 2 steps

1: 7 percent / DEPC, Et₃N / tetrahydrofuran / 16 h / 20 °C

2: 1.) S₂Cl₂, 2.) NaBH₄, 3.) aq. H₂O₂

With disulfur dichloride; sodium tetrahydroborate; dihydrogen peroxide; triethylamine; diethyl dicarbonate; In tetrahydrofuran;
DOI:10.1021/jm00031a009

Reference yield:

: 6232-11-7
methyl 4-(aminomethyl)benzoate hydrochloride

: 153408-50-5
2,2'-dithiobismethyl>-1H-indole-3-propanamide>

Guidance literature:: Multi-step reaction with 2 steps

1: 7 percent / DEPC, Et₃N / tetrahydrofuran / 16 h / 20 °C

2: 1.) S₂Cl₂, 2.) NaBH₄, 3.) aq. H₂O₂

With disulfur dichloride; sodium tetrahydroborate; dihydrogen peroxide; triethylamine; diethyl dicarbonate; In tetrahydrofuran;
DOI:10.1021/jm00031a009

Reference yield:

: 153408-77-6
N-(4-methoxycarbonylbenzyl)-3-(3-indolyl)propanamide

: C₄₀H₃₈N₄O₆S

: 153408-50-5
2,2'-dithiobismethyl>-1H-indole-3-propanamide>

Guidance literature:: With disulfur dichloride; sodium tetrahydroborate; dihydrogen peroxide; Yield given. Multistep reaction. Yields of byproduct given;
DOI:10.1021/jm00031a009