carbonic acid 4-chlorocarbonylmethyl-2-methoxycarbonyloxy-phenyl ester methyl ester

Base Information

Chemical Name:carbonic acid 4-chlorocarbonylmethyl-2-methoxycarbonyloxy-phenyl ester methyl ester
CAS No.:244612-70-2
Molecular Formula:C₁₂H₁₁ClO₇
Molecular Weight:302.668
Hs Code.:

Synonyms:carbonic acid 4-chlorocarbonylmethyl-2-methoxycarbonyloxy-phenyl ester methyl ester

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Chemical Property of carbonic acid 4-chlorocarbonylmethyl-2-methoxycarbonyloxy-phenyl ester methyl ester

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Technology Process of carbonic acid 4-chlorocarbonylmethyl-2-methoxycarbonyloxy-phenyl ester methyl ester

There total 2 articles about carbonic acid 4-chlorocarbonylmethyl-2-methoxycarbonyloxy-phenyl ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 222320-70-9
3,4-bis(methoxycarbonyloxy)-phenylacetic acid

: 244612-70-2
carbonic acid 4-chlorocarbonylmethyl-2-methoxycarbonyloxy-phenyl ester methyl ester

Guidance literature:: With oxalyl dichloride; for 1h; Ambient temperature;
DOI:10.1021/jm9804735

Reference yield:

: 102-32-9
3,4-dihydroxyphenylacetate

: 244612-70-2
carbonic acid 4-chlorocarbonylmethyl-2-methoxycarbonyloxy-phenyl ester methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1N aq. NaOH / 0 °C

2: oxalyl chloride / 1 h / Ambient temperature

With sodium hydroxide; oxalyl dichloride;
DOI:10.1021/jm9804735

Reference yield:

: 244612-70-2
carbonic acid 4-chlorocarbonylmethyl-2-methoxycarbonyloxy-phenyl ester methyl ester

: bis(3,5-dihydroxyphenylacetyl)-L-tartaric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) 80 percent aq. HOAc / 1.) 135 - 160 deg C, 2.) reflux, 30 min

2: 2 percent aq. Na₂CO₃ / tetrahydrofuran; methanol

With sodium carbonate; acetic acid; In tetrahydrofuran; methanol;
DOI:10.1021/jm9804735