C₃₂H₅₆O₈S₂Si

Base Information

Chemical Name:C₃₂H₅₆O₈S₂Si
CAS No.:934617-99-9
Molecular Formula:C₃₂H₅₆O₈S₂Si
Molecular Weight:661.009
Hs Code.:

C<sub>32</sub>H<sub>56</sub>O<sub>8</sub>S<sub>2</sub>Si

Synonyms:C₃₂H₅₆O₈S₂Si

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Chemical Property of C₃₂H₅₆O₈S₂Si

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Technology Process of C₃₂H₅₆O₈S₂Si

There total 9 articles about C₃₂H₅₆O₈S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 934617-98-8
C₃₈H₇₀O₈S₂Si₂

: 934617-99-9
C₃₂H₅₆O₈S₂Si

Guidance literature:: With water; acetic acid; In tetrahydrofuran; at 50 ℃;
DOI:10.1246/cl.2007.278

Reference yield:

: C₁₃H₁₆O₃

: 934617-99-9
C₃₂H₅₆O₈S₂Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: H₂ / Pd/C / ethyl acetate

2.1: 71 percent / Mg; HgCl₂ / diethyl ether / -50 - -15 °C

3.1: 100 percent / 2,6-lutidine / CH₂Cl₂

4.1: ZnI₂; n-Bu₄NI / 1,2-dichloro-ethane

4.2: Ac₂O; AcOH / dimethylsulfoxide / 70 °C

5.1: 92 percent / n-BuLi; BF₃*OEt₂ / tetrahydrofuran / -78 °C

6.1: 100 percent / TEA; DMAP / CH₂Cl₂

7.1: 94 percent / AcOH; H₂O / tetrahydrofuran / 50 °C

With 2,6-dimethylpyridine; dmap; n-butyllithium; TEA; boron trifluoride diethyl etherate; water; hydrogen; tetra-(n-butyl)ammonium iodide; magnesium; acetic acid; mercury dichloride; zinc(II) iodide; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1246/cl.2007.278

Reference yield:

: 102490-00-6
(2S,3R)-1,2-epoxy-4-penten-3-ol

: 934617-99-9
C₃₂H₅₆O₈S₂Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: i-Pr₂NEt; n-Bu₄NI / 1,2-dichloro-ethane / 50 °C

2.1: H₂ / Pd/C / ethyl acetate

3.1: 71 percent / Mg; HgCl₂ / diethyl ether / -50 - -15 °C

4.1: 100 percent / 2,6-lutidine / CH₂Cl₂

5.1: ZnI₂; n-Bu₄NI / 1,2-dichloro-ethane

5.2: Ac₂O; AcOH / dimethylsulfoxide / 70 °C

6.1: 92 percent / n-BuLi; BF₃*OEt₂ / tetrahydrofuran / -78 °C

7.1: 100 percent / TEA; DMAP / CH₂Cl₂

8.1: 94 percent / AcOH; H₂O / tetrahydrofuran / 50 °C

With 2,6-dimethylpyridine; dmap; n-butyllithium; TEA; boron trifluoride diethyl etherate; water; hydrogen; tetra-(n-butyl)ammonium iodide; magnesium; acetic acid; N-ethyl-N,N-diisopropylamine; mercury dichloride; zinc(II) iodide; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1246/cl.2007.278