α-isopropylcyclohexaneacetic acid

Base Information

Chemical Name:α-isopropylcyclohexaneacetic acid
CAS No.:19986-15-3
Molecular Formula:C₁₁H₂₀O₂
Molecular Weight:184.279
Hs Code.:

Synonyms:α-isopropylcyclohexaneacetic acid

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Chemical Property of α-isopropylcyclohexaneacetic acid

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Technology Process of α-isopropylcyclohexaneacetic acid

There total 4 articles about α-isopropylcyclohexaneacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 351874-87-8
α-iso-propylcyclohexaneacetic acid methyl ester

: 19986-15-3
α-isopropylcyclohexaneacetic acid

Guidance literature:: With boron tribromide; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/S0957-4166(01)00114-8

Reference yield:

: 72615-27-1
2-phenyl-3-methylbutyric acid methyl ester

: 19986-15-3
α-isopropylcyclohexaneacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / Rh/Al₂O₃ / 2-methyl-propan-2-ol / 50 h / 20 °C

2: 46 percent / BBr₃ / CH₂Cl₂ / 2 h / 20 °C

With hydrogen; boron tribromide; Rh/Al₂O₃; In dichloromethane; tert-butyl alcohol;
DOI:10.1016/S0957-4166(01)00114-8

Reference yield:

: 101-41-7
benzeneacetic acid methyl ester

: 19986-15-3
α-isopropylcyclohexaneacetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / LDA; HMPA / tetrahydrofuran / -78 °C

2: 100 percent / H₂ / Rh/Al₂O₃ / 2-methyl-propan-2-ol / 50 h / 20 °C

3: 46 percent / BBr₃ / CH₂Cl₂ / 2 h / 20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; hydrogen; boron tribromide; lithium diisopropyl amide; Rh/Al₂O₃; In tetrahydrofuran; dichloromethane; tert-butyl alcohol;
DOI:10.1016/S0957-4166(01)00114-8