[5,15-diethynyl-10,20-bis(2',6'-bis(3,3-dimethyl-1-butyloxy)phenyl)porphinato]zinc(II)

Base Information

Chemical Name:[5,15-diethynyl-10,20-bis(2',6'-bis(3,3-dimethyl-1-butyloxy)phenyl)porphinato]zinc(II)
CAS No.:478184-35-9
Molecular Formula:C₆₀H₆₈N₄O₄Zn
Molecular Weight:974.614
Hs Code.:

Synonyms:[5,15-diethynyl-10,20-bis(2',6'-bis(3,3-dimethyl-1-butyloxy)phenyl)porphinato]zinc(II)

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Chemical Property of [5,15-diethynyl-10,20-bis(2',6'-bis(3,3-dimethyl-1-butyloxy)phenyl)porphinato]zinc(II)

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Technology Process of [5,15-diethynyl-10,20-bis(2',6'-bis(3,3-dimethyl-1-butyloxy)phenyl)porphinato]zinc(II)

There total 1 articles about [5,15-diethynyl-10,20-bis(2',6'-bis(3,3-dimethyl-1-butyloxy)phenyl)porphinato]zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 731794-60-8
[5,15-bis(trimethylsilylethynyl)-10,20-bis(2',6'-bis(3,3-dimethyl-1-butyloxy)phenyl)porphinato]zinc(II)

: 478184-35-9
[5,15-diethynyl-10,20-bis(2',6'-bis(3,3-dimethyl-1-butyloxy)phenyl)porphinato]zinc(II)

Guidance literature:: [5,15-bis(trimethylsilylethynyl)-10,20-bis(2',6'-bis(3,3-dimethyl-1-butyloxy)phenyl)porphinato]zinc(II); With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 0.0833333h;

With water; In tetrahydrofuran;

Reference yield: 98.0%

: 478184-35-9
[5,15-diethynyl-10,20-bis(2',6'-bis(3,3-dimethyl-1-butyloxy)phenyl)porphinato]zinc(II)

: 944245-13-0
4-(4-(N,N-dihexylamino)phenylethynyl)-7-iodobenzo[c][1,2,5]thiadiazole

: C₁₁₂H₁₃₀N₁₀O₄S₂Zn

Guidance literature:: With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 49 ℃; for 20h; Inert atmosphere;
DOI:10.1142/S1088424614501107

Reference yield: 91.0%

: ammonium hexafluorophosphate

: osmium(II) (4'-bromo-2,2';6',2''-terpyridinyl)(2,2';6',2''-terpyridinyl) bis(hexafluorophosphate)

: 478184-35-9
[5,15-diethynyl-10,20-bis(2',6'-bis(3,3-dimethyl-1-butyloxy)phenyl)porphinato]zinc(II)

: bisosmium(II) 5,15-bis[4'-ethynyl-(2,2';6',2-terpyridinyl)]bis[10,20-di(2',6'-bis(3,3-dimethylbutoxy)phenyl)porphinato]zinc(II)-bis(2,2';6',2-terpyridine)4+ tetrakis-hexafluorophosphate

Guidance literature:: osmium(II) (4'-bromo-2,2';6',2''-terpyridinyl)(2,2';6',2''-terpyridinyl) bis(hexafluorophosphate); [5,15-diethynyl-10,20-bis(2',6'-bis(3,3-dimethyl-1-butyloxy)phenyl)porphinato]zinc(II); With copper(l) iodide; diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; acetonitrile;

ammonium hexafluorophosphate; In water; acetonitrile;