3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-O²,2'-cyclouridine

Base Information

• Chemical Name: 3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-O²,2'-cyclouridine
• CAS No.: 88121-27-1
• Molecular Formula: C₂₁H₃₆N₂O₆Si₂
• Molecular Weight: 468.698

Synonyms:3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-O²,2'-cyclouridine

Chemical Property of 3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-O²,2'-cyclouridine

Chemical Property:

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Technology Process of 3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-O²,2'-cyclouridine

There total 1 articles about 3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-O²,2'-cyclouridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

Trifluoro-methanesulfonic acid (2R,3R,3aR,9aR)-2-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-3-yl ester → N3,O2'-dibenzoyl-3',5'-O-TIPDS-uridine (151507-67-4) + 3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-O2,2'-cyclouridine (88121-27-1)

Guidance literature:

With dmap; triethylamine; In chloroform-d1; for 4h;

DOI:10.1016/S0040-4039(98)01616-5

Reference yield: 53.0%

diphenyl diselenide (1666-13-3) + 3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-O2,2'-cyclouridine (88121-27-1) → 3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-2'-deoxy-2'-phenylselenouridine (503043-95-6)

Guidance literature:

diphenyl diselenide; With lithium aluminium tetrahydride; In 1,4-dioxane;

3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-O²,2'-cyclouridine; In 1,4-dioxane; at 20 ℃; Further stages.;

DOI:10.1021/jo020620d

Downstream raw materials:

3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-2'-deoxy-2'-phenylselenouridine

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