N-acetyl dehydrophenylalanyl-(S)-phenylalanine

Base Information

Chemical Name:N-acetyl dehydrophenylalanyl-(S)-phenylalanine
CAS No.:42291-22-5
Molecular Formula:C₂₀H₂₀N₂O₄
Molecular Weight:352.39
Hs Code.:

Synonyms:N-acetyl dehydrophenylalanyl-(S)-phenylalanine

Suppliers and Price of N-acetyl dehydrophenylalanyl-(S)-phenylalanine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-acetyl dehydrophenylalanyl-(S)-phenylalanine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-acetyl dehydrophenylalanyl-(S)-phenylalanine

There total 2 articles about N-acetyl dehydrophenylalanyl-(S)-phenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 55065-02-6,64590-80-3,5469-45-4
N-acetamido cinnamic acid

: 42291-22-5,78087-67-9,78087-68-0,80226-20-6,82597-38-4,97275-08-6
2-((Z)-2-Acetylamino-3-phenyl-acryloylamino)-3-phenyl-propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 3 h / 90 °C

2: 2N NaOH / acetone; H₂O / 0 deg C, 20 min, pH: 9-11, then rt., 30 min

With sodium hydroxide; thionyl chloride; In water; acetone;
DOI:10.1248/cpb.36.4426

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 120681-11-0
(Z)-2-Acetylamino-3-phenyl-acryloyl chloride

: 42291-22-5,78087-67-9,78087-68-0,80226-20-6,82597-38-4,97275-08-6
2-((Z)-2-Acetylamino-3-phenyl-acryloylamino)-3-phenyl-propionic acid

Guidance literature:: With sodium hydroxide; In water; acetone; 0 deg C, 20 min, pH: 9-11, then rt., 30 min;
DOI:10.1248/cpb.36.4426

Reference yield: 21.0%

: 42291-22-5
N-acetyl dehydrophenylalanyl-(S)-phenylalanine

: 10030-31-6
(S)-2-((S)-2-acetamido-3-phenylpropanamido)-3-phenylpropanoic acid

: 24809-18-5
Ac-D-Phe-L-Phe-OH

Guidance literature:: With hydrogen; Rh(I)-chiral diphosphinite; In ethanol; at 20 ℃; for 45h; Title compound not separated from byproducts; other chiral diphosphinite, other time;
DOI:10.1246/bcsj.57.739