Technology Process of C40H54N4O10S2
There total 1 articles about C40H54N4O10S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
DOI:10.1039/b311583f
- Guidance literature:
-
Multi-step reaction with 5 steps
1: aq. TFA / CH2Cl2
2: 68 percent / DTT; guanidinium hydrochloride / various solvent(s) / 20 °C / pH 8.0
3: 65 percent / aq. Na2CO3 / dimethylformamide
4: 94 percent / H2 / Pd/C / ethyl acetate; ethanol
5: 88 percent / PyBOP; DIPEA / dimethylformamide
With
DL-dithiothreitol; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; guanidine hydrochloride; sodium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
palladium on activated charcoal;
In
ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/b311583f
- Guidance literature:
-
Multi-step reaction with 7 steps
1: aq. TFA / CH2Cl2
2: 68 percent / DTT; guanidinium hydrochloride / various solvent(s) / 20 °C / pH 8.0
3: 65 percent / aq. Na2CO3 / dimethylformamide
4: 94 percent / H2 / Pd/C / ethyl acetate; ethanol
5: 88 percent / PyBOP; DIPEA / dimethylformamide
6: 85 percent / H2 / Pd/C / ethyl acetate; ethanol
7: 85 percent / PyBOP; DIPEA / dimethylformamide
With
DL-dithiothreitol; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; guanidine hydrochloride; sodium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
palladium on activated charcoal;
In
ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/b311583f