methyl 2,2-ethylenedioxypropyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate

Base Information

Chemical Name:methyl 2,2-ethylenedioxypropyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate
CAS No.:86780-86-1
Molecular Formula:C₂₁H₂₄N₂O₈
Molecular Weight:432.43
Hs Code.:

Synonyms:methyl 2,2-ethylenedioxypropyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate

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Chemical Property of methyl 2,2-ethylenedioxypropyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate

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Technology Process of methyl 2,2-ethylenedioxypropyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate

There total 6 articles about methyl 2,2-ethylenedioxypropyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 86780-86-1
methyl 2,2-ethylenedioxypropyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate

Guidance literature:

Reference yield: 40.0%

: 39562-17-9
methyl 2-(3-nitrophenylmethylene)acetoacetate

: 86780-81-6
3-amino-2-crotonic acid 2,2-ethylenedioxy propyl ester

: 86780-86-1
methyl 2,2-ethylenedioxypropyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate

Guidance literature:: In ethanol; Heating;
DOI:10.1248/cpb.34.1589

Reference yield:

: 10004-17-8
(2-methyl-[1,3]dioxolan-2-yl)-methanol

: 86780-86-1
methyl 2,2-ethylenedioxypropyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / 60percent NaH in oil / 2 h / 70 - 80 °C

2: 84 percent / NH₃ / methanol / 2.5 h / 0 - 5 °C

3: 40 percent / ethanol / Heating

With ammonia; sodium hydride; In methanol; ethanol;
DOI:10.1248/cpb.34.1589