C₂₅H₂₆N₆O₅

Base Information

Chemical Name:C₂₅H₂₆N₆O₅
CAS No.:1300590-14-0
Molecular Formula:C₂₅H₂₆N₆O₅
Molecular Weight:490.519
Hs Code.:

C<sub>25</sub>H<sub>26</sub>N<sub>6</sub>O<sub>5</sub>

Synonyms:C₂₅H₂₆N₆O₅

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Chemical Property of C₂₅H₂₆N₆O₅

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Technology Process of C₂₅H₂₆N₆O₅

There total 8 articles about C₂₅H₂₆N₆O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1300590-12-8
C₃₄H₂₉F₃N₆O₇

: 1300590-14-0
C₂₅H₂₆N₆O₅

Guidance literature:: With ammonia; water; In methanol; at 20 ℃; for 19h;

Reference yield:

: 3,5-di-O-benzyl-4-C-(tert-butyldiphenylsilyloxymethyl)-1,2-O-isopropylidene-α-D-ribofuranose

: 1300590-14-0
C₂₅H₂₆N₆O₅

Guidance literature:: Multi-step reaction with 13 steps

1: sulfuric acid; acetic acid / 3.5 h

2: N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate / acetonitrile / 1 h / 20 °C / Inert atmosphere; Reflux

3: methylamine / water; tetrahydrofuran / 0.5 h / 20 °C

4: dmap; trifluoromethane sulfonyl chloride / dichloromethane / 1 h / 20 °C / Inert atmosphere; Cooling with ice

5: sodium hydroxide; water / tetrahydrofuran / 1.5 h / 20 °C

6: pyridine / dichloromethane / 1 h / Inert atmosphere; Cooling with ice

7: sodium azide / N,N-dimethyl-formamide / 48 h / Inert atmosphere

8: water; tributylphosphine / tetrahydrofuran / 8 h / 20 °C / Inert atmosphere

9: pyridine / dichloromethane / 0.5 h / Inert atmosphere

10: N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate / 1,2-dichloro-ethane / 3.5 h / Inert atmosphere; Reflux

11: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 20 °C / Inert atmosphere

12: dipyridinium dichromate / N,N-dimethyl-formamide / 17 h / 20 °C / Inert atmosphere; Molecular sieve

13: water; ammonia / methanol / 19 h / 20 °C

With pyridine; dmap; dipyridinium dichromate; sodium azide; N,O-bis-(trimethylsilyl)-acetamide; tributylphosphine; trifluoromethane sulfonyl chloride; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; tetrabutyl ammonium fluoride; ammonia; water; acetic acid; methylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1300589-63-2
2'-O-acetyl-3',5'-di-O-benzyl-4'-C-(tert-butyldiphenylsilyloxymethyl)-5-methyluridine

: 1300590-14-0
C₂₅H₂₆N₆O₅

Guidance literature:: Multi-step reaction with 11 steps

1: methylamine / water; tetrahydrofuran / 0.5 h / 20 °C

2: dmap; trifluoromethane sulfonyl chloride / dichloromethane / 1 h / 20 °C / Inert atmosphere; Cooling with ice

3: sodium hydroxide; water / tetrahydrofuran / 1.5 h / 20 °C

4: pyridine / dichloromethane / 1 h / Inert atmosphere; Cooling with ice

5: sodium azide / N,N-dimethyl-formamide / 48 h / Inert atmosphere

6: water; tributylphosphine / tetrahydrofuran / 8 h / 20 °C / Inert atmosphere

7: pyridine / dichloromethane / 0.5 h / Inert atmosphere

8: N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate / 1,2-dichloro-ethane / 3.5 h / Inert atmosphere; Reflux

9: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 20 °C / Inert atmosphere

10: dipyridinium dichromate / N,N-dimethyl-formamide / 17 h / 20 °C / Inert atmosphere; Molecular sieve

11: water; ammonia / methanol / 19 h / 20 °C

With pyridine; dmap; dipyridinium dichromate; sodium azide; N,O-bis-(trimethylsilyl)-acetamide; tributylphosphine; trifluoromethane sulfonyl chloride; trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; ammonia; water; methylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;