3'-<(acetylamino)propyl>-3,5-diiodo-N-(trifluoroacetyl)-O-methylthyronine methyl ester

Base Information

Chemical Name:3'-<(acetylamino)propyl>-3,5-diiodo-N-(trifluoroacetyl)-O-methylthyronine methyl ester
CAS No.:111088-55-2
Molecular Formula:C₂₄H₂₅F₃I₂N₂O₆
Molecular Weight:748.277
Hs Code.:

Synonyms:3'-<(acetylamino)propyl>-3,5-diiodo-N-(trifluoroacetyl)-O-methylthyronine methyl ester

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Chemical Property of 3'-<(acetylamino)propyl>-3,5-diiodo-N-(trifluoroacetyl)-O-methylthyronine methyl ester

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Technology Process of 3'-<(acetylamino)propyl>-3,5-diiodo-N-(trifluoroacetyl)-O-methylthyronine methyl ester

There total 3 articles about 3'-<(acetylamino)propyl>-3,5-diiodo-N-(trifluoroacetyl)-O-methylthyronine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 93800-45-4
N-trifluoroacetyl-3,5-diiodo-L-tyrosine methyl ester

: 111088-48-3
Bis-[3-(3-acetylamino-propyl)-4-methoxy-phenyl]-iodonium; bromide

: 111088-55-2
3'-<(acetylamino)propyl>-3,5-diiodo-N-(trifluoroacetyl)-O-methylthyronine methyl ester

Guidance literature:: With copper; triethylamine; In methanol;
DOI:10.1021/jm00396a008

Reference yield:

: 18655-51-1
2-(3-Aminopropyl)-1-methoxybenzene

: 111088-55-2
3'-<(acetylamino)propyl>-3,5-diiodo-N-(trifluoroacetyl)-O-methylthyronine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: H₂O / 1 h

2: iodine tris(trifluoroacetate), NaBr

3: 35 percent / Cu, Et₃N / methanol

With iodine tris(trifluoroacetate); copper; triethylamine; sodium bromide; In methanol; water;
DOI:10.1021/jm00396a008

Reference yield:

: 111088-41-6
N-acetyl-3-(2-methoxyphenyl)propanamine

: 111088-55-2
3'-<(acetylamino)propyl>-3,5-diiodo-N-(trifluoroacetyl)-O-methylthyronine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: iodine tris(trifluoroacetate), NaBr

2: 35 percent / Cu, Et₃N / methanol

With iodine tris(trifluoroacetate); copper; triethylamine; sodium bromide; In methanol;
DOI:10.1021/jm00396a008