tert-butyl (1S,3S)-1-(3,4-dimethoxyphenyl)-3-hydroxy hex-5-enylcarbamate

Base Information

Chemical Name:tert-butyl (1S,3S)-1-(3,4-dimethoxyphenyl)-3-hydroxy hex-5-enylcarbamate
CAS No.:1162664-67-6
Molecular Formula:C₁₉H₂₉NO₅
Molecular Weight:351.443
Hs Code.:

Synonyms:tert-butyl (1S,3S)-1-(3,4-dimethoxyphenyl)-3-hydroxy hex-5-enylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl (1S,3S)-1-(3,4-dimethoxyphenyl)-3-hydroxy hex-5-enylcarbamate

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Technology Process of tert-butyl (1S,3S)-1-(3,4-dimethoxyphenyl)-3-hydroxy hex-5-enylcarbamate

There total 2 articles about tert-butyl (1S,3S)-1-(3,4-dimethoxyphenyl)-3-hydroxy hex-5-enylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: [1-(3,4-dimethoxy-phenyl)-3-oxo-propyl]-carbamic acid tert-butyl ester

: 24850-33-7
allyltributylstanane

: 1162664-67-6
tert-butyl (1S,3S)-1-(3,4-dimethoxyphenyl)-3-hydroxy hex-5-enylcarbamate

Guidance literature:: With (S,S)-biphenyl-titanium complex; In dichloromethane; water; at -15 - 0 ℃; for 24h; optical yield given as %ee; enantioselective reaction;
DOI:10.1016/j.tetlet.2009.07.128