2,4-Bis-tert-butoxycarbonyl-3-methoxycarbonyl-pentanedioic acid di-tert-butyl ester

Base Information

Chemical Name:2,4-Bis-tert-butoxycarbonyl-3-methoxycarbonyl-pentanedioic acid di-tert-butyl ester
CAS No.:87376-40-7
Molecular Formula:C₂₅H₄₂O₁₀
Molecular Weight:502.602
Hs Code.:

Synonyms:2,4-Bis-tert-butoxycarbonyl-3-methoxycarbonyl-pentanedioic acid di-tert-butyl ester

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Chemical Property of 2,4-Bis-tert-butoxycarbonyl-3-methoxycarbonyl-pentanedioic acid di-tert-butyl ester

Chemical Property:

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Technology Process of 2,4-Bis-tert-butoxycarbonyl-3-methoxycarbonyl-pentanedioic acid di-tert-butyl ester

There total 2 articles about 2,4-Bis-tert-butoxycarbonyl-3-methoxycarbonyl-pentanedioic acid di-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 541-16-2
t-butyl malonate

: 64356-76-9
N-benzyloxycarbonyl α-chloro glycine methyl ester

: 621-84-1
O-benzyl carbamate

: 2-tert-Butoxycarbonyl-but-2-enedioic acid 1-tert-butyl ester 4-methyl ester

: 87376-40-7
2,4-Bis-tert-butoxycarbonyl-3-methoxycarbonyl-pentanedioic acid di-tert-butyl ester

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) THF, r. t., 2.) THF, 16 h;
DOI:10.1016/S0040-4039(00)81741-4

Reference yield:

: 541-16-2
t-butyl malonate

: 64356-76-9
N-benzyloxycarbonyl α-chloro glycine methyl ester

: 621-84-1
O-benzyl carbamate

: 87376-41-8
2-Benzyloxycarbonylamino-3-tert-butoxycarbonyl-succinic acid 4-tert-butyl ester 1-methyl ester

: 87376-40-7
2,4-Bis-tert-butoxycarbonyl-3-methoxycarbonyl-pentanedioic acid di-tert-butyl ester

Guidance literature:: With sodium hydride; triethylamine; Yield given. Multistep reaction; 1.) THF, 6 h, 2.) THF, 1.5 h;
DOI:10.1016/S0040-4039(00)81741-4