C₂₇H₅₀O₃Si₂

Base Information

Chemical Name:C₂₇H₅₀O₃Si₂
CAS No.:1258500-86-5
Molecular Formula:C₂₇H₅₀O₃Si₂
Molecular Weight:478.863
Hs Code.:

C<sub>27</sub>H<sub>50</sub>O<sub>3</sub>Si<sub>2</sub>

Synonyms:C₂₇H₅₀O₃Si₂

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Chemical Property of C₂₇H₅₀O₃Si₂

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Technology Process of C₂₇H₅₀O₃Si₂

There total 9 articles about C₂₇H₅₀O₃Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1258500-85-4
C₂₄H₄₄O₃Si₂

: 64503-52-2
tetraisopropenyltin

: 1258500-86-5
C₂₇H₅₀O₃Si₂

Guidance literature:: tetraisopropenyltin; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 0.166667h; Inert atmosphere;

C₂₄H₄₄O₃Si₂; In tetrahydrofuran; hexane; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1002/chem.201001813

Reference yield: 98.0%

: 6386-71-6
isopropenyllithium

: 1258500-85-4
C₂₄H₄₄O₃Si₂

: 1258500-86-5
C₂₇H₅₀O₃Si₂

Guidance literature:: DOI:10.1021/jo2019027

Reference yield:

: 1258500-80-9
C₂₅H₃₃NO₄Si

: 1258500-86-5
C₂₇H₅₀O₃Si₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.33 h / -78 °C

1.2: -78 - 5 °C

2.1: water; dihydrogen peroxide; lithium hydroxide / tetrahydrofuran / 0.17 h / 20 °C

3.1: dmap; 1,1'-carbonyldiimidazole / dichloromethane / 1 h / 0 °C

4.1: ozone / methanol / 0.05 h / -78 °C

5.1: sodium tetrahydroborate / 20 °C

6.1: 1H-imidazole / N,N-dimethyl-formamide / 12 h / 20 °C

7.1: tetrahydrofuran / 1 h / 0 °C

With 1H-imidazole; dmap; sodium tetrahydroborate; water; dihydrogen peroxide; ozone; 1,1'-carbonyldiimidazole; lithium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo2019027