(Z)-3-[1-(3-fluoro-6H-dibenzo[b,e]oxepin-11-ylidene)-ethyl]-nitrobenzene

Base Information

Chemical Name:(Z)-3-[1-(3-fluoro-6H-dibenzo[b,e]oxepin-11-ylidene)-ethyl]-nitrobenzene
CAS No.:886862-14-2
Molecular Formula:C₂₂H₁₆FNO₃
Molecular Weight:361.372
Hs Code.:

Synonyms:(Z)-3-[1-(3-fluoro-6H-dibenzo[b,e]oxepin-11-ylidene)-ethyl]-nitrobenzene

Suppliers and Price of (Z)-3-[1-(3-fluoro-6H-dibenzo[b,e]oxepin-11-ylidene)-ethyl]-nitrobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-3-[1-(3-fluoro-6H-dibenzo[b,e]oxepin-11-ylidene)-ethyl]-nitrobenzene

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Technology Process of (Z)-3-[1-(3-fluoro-6H-dibenzo[b,e]oxepin-11-ylidene)-ethyl]-nitrobenzene

There total 2 articles about (Z)-3-[1-(3-fluoro-6H-dibenzo[b,e]oxepin-11-ylidene)-ethyl]-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5159-41-1
2-iodobenzyl alcohol

: 886862-14-2
(Z)-3-[1-(3-fluoro-6H-dibenzo[b,e]oxepin-11-ylidene)-ethyl]-nitrobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: diethylamine / bis(triphenylphosphine)palladium(II) chloride; copper(I) iodide / 12 h / 20 °C

2: 74 percent / triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 12 h / 20 °C

3: 77 percent / sodium carbonate / Pd(OAc)2 / dioxane; H₂O / 12 h / 70 °C

With di-isopropyl azodicarboxylate; sodium carbonate; diethylamine; triphenylphosphine; palladium diacetate; copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; In tetrahydrofuran; 1,4-dioxane; water; 1: Sonogashira coupling / 2: Mitsunobu reaction;
DOI:10.1021/ol060289a

Reference yield:

: 210964-23-1
1-hydroxymethyl-2-(1-propyn-1-yl)-benzene

: 886862-14-2
(Z)-3-[1-(3-fluoro-6H-dibenzo[b,e]oxepin-11-ylidene)-ethyl]-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 12 h / 20 °C

2: 77 percent / sodium carbonate / Pd(OAc)2 / dioxane; H₂O / 12 h / 70 °C

With di-isopropyl azodicarboxylate; sodium carbonate; triphenylphosphine; palladium diacetate; In tetrahydrofuran; 1,4-dioxane; water; 1: Mitsunobu reaction;
DOI:10.1021/ol060289a