dicarbonylmethyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium⁽¹⁺⁾ hexafluorophosphate

Base Information

• Chemical Name: dicarbonylmethyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium⁽¹⁺⁾ hexafluorophosphate
• CAS No.: 99299-50-0
• Molecular Formula: C₄₄H₄₂O₂P₃Ru*F₆P
• Molecular Weight: 941.772

Synonyms:dicarbonylmethyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium⁽¹⁺⁾ hexafluorophosphate

Chemical Property of dicarbonylmethyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium⁽¹⁺⁾ hexafluorophosphate

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of dicarbonylmethyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium⁽¹⁺⁾ hexafluorophosphate

There total 2 articles about dicarbonylmethyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium⁽¹⁺⁾ hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

sodium hexaflorophosphate + dicarbonyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium(0) (37843-33-7) → dicarbonylmethyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium(1+) hexafluorophosphate (99299-50-0)

Guidance literature:

With methyl iodide; In ethanol; dichloromethane; under N2, Ru(CO)2(triphos) in CH2Cl2 treated with MeI, stirred at room temp. for 30 min, hexane added, ppt. treated with NaPF6 in EtOH; ppt. collected, washed with EtOH and Et2O, dried in vac. at 80°C; elem. anal.;

Reference yield:

RuCH3(CO)(P(CH3)2C6H5)(C41H39P3)(1+)*PF6(1-)=[RuCH3(CO)(P(CH3)2C6H5)(C41H39P3)]PF6 (102283-22-7) → dicarbonylmethyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium(1+) hexafluorophosphate (99299-50-0)

Guidance literature:

With CO; In chloroform-d1; High Pressure; 380 psi CO, 2 d;

DOI:10.1021/om00138a014

upstream raw materials:

dicarbonyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium⁽⁰⁾

RuCH₃(CO)(P(CH₃)2C₆H₅)(C₄₁H₃₉P₃)⁽¹⁺⁾*PF₆^(1-)=[RuCH₃(CO)(P(CH₃)2C₆H₅)(C₄₁H₃₉P₃)]PF₆

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