tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-1-O-trichloroacetimidoyl-α-D-glucopyranosyl)uronate

Base Information

Chemical Name:tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-1-O-trichloroacetimidoyl-α-D-glucopyranosyl)uronate
CAS No.:1253183-63-9
Molecular Formula:C₃₃H₃₄Cl₃NO₈
Molecular Weight:678.994
Hs Code.:

Synonyms:tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-1-O-trichloroacetimidoyl-α-D-glucopyranosyl)uronate

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Chemical Property of tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-1-O-trichloroacetimidoyl-α-D-glucopyranosyl)uronate

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Technology Process of tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-1-O-trichloroacetimidoyl-α-D-glucopyranosyl)uronate

There total 1 articles about tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-1-O-trichloroacetimidoyl-α-D-glucopyranosyl)uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tert-butyl (ethyl 3,4-di-O-benzyl-2-O-benzoyl-1-thio-β-D-glucopyranosid)uronate

: 545-06-2
trichloroacetonitrile

: 1253183-63-9
tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-1-O-trichloroacetimidoyl-α-D-glucopyranosyl)uronate

Guidance literature:: tert-butyl (ethyl 3,4-di-O-benzyl-2-O-benzoyl-1-thio-β-D-glucopyranosid)uronate; With N-Bromosuccinimide; In water; acetonitrile; at 0 - 20 ℃;

trichloroacetonitrile; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tet.2010.08.004

Reference yield: 89.0%

: 1253183-63-9
tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-1-O-trichloroacetimidoyl-α-D-glucopyranosyl)uronate

: 277756-87-3
phenyl 2-azido-3,6-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside

: 1253183-67-3
phenyl [tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside)

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In toluene; at -30 ℃; for 1.5h; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.tet.2010.08.004