dimethyl <<4-<(p-amidino-N-methylbenzamido)acetyl>-o-phenylene>dioxy>diacetate

Base Information

Chemical Name:dimethyl <<4-<(p-amidino-N-methylbenzamido)acetyl>-o-phenylene>dioxy>diacetate
CAS No.:132224-05-6
Molecular Formula:C₂₃H₂₅N₃O₈
Molecular Weight:471.467
Hs Code.:

Synonyms:dimethyl <<4-<(p-amidino-N-methylbenzamido)acetyl>-o-phenylene>dioxy>diacetate

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Chemical Property of dimethyl <<4-<(p-amidino-N-methylbenzamido)acetyl>-o-phenylene>dioxy>diacetate

Chemical Property:

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Technology Process of dimethyl <<4-<(p-amidino-N-methylbenzamido)acetyl>-o-phenylene>dioxy>diacetate

There total 6 articles about dimethyl <<4-<(p-amidino-N-methylbenzamido)acetyl>-o-phenylene>dioxy>diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1025821-85-5
(2-Methoxycarbonylmethoxy-5-{2-[methyl-(4-methylsulfanylcarbonimidoyl-benzoyl)-amino]-acetyl}-phenoxy)-acetic acid methyl ester

: 132224-05-6
dimethyl <<4-<(p-amidino-N-methylbenzamido)acetyl>-o-phenylene>dioxy>diacetate

Guidance literature:: With ammonium acetate; In methanol; at 70 ℃;
DOI:10.1021/jm00101a017

Reference yield:

: 62-13-5
1-(3,4-dihydroxyphenyl)-1-oxo-2-methylamino-ethan-hydrochlorid

: 132224-05-6
dimethyl <<4-<(p-amidino-N-methylbenzamido)acetyl>-o-phenylene>dioxy>diacetate

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / pyridine / 2 h / Ambient temperature

2: 60 percent / K₂CO₃ / dimethylformamide / 2 h / 50 - 60 °C

3: H₂S, triethylamine (TEA) / pyridine / Ambient temperature

4: acetone / 50 °C

5: ammonium acetate / methanol / 70 °C

With pyridine; ammonium acetate; hydrogen sulfide; potassium carbonate; triethylamine; In pyridine; methanol; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm00101a017

Reference yield:

: 6068-72-0
4-cyanobenzoyl chlorIde

: 132224-05-6
dimethyl <<4-<(p-amidino-N-methylbenzamido)acetyl>-o-phenylene>dioxy>diacetate

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / pyridine / 2 h / Ambient temperature

2: 60 percent / K₂CO₃ / dimethylformamide / 2 h / 50 - 60 °C

3: H₂S, triethylamine (TEA) / pyridine / Ambient temperature

4: acetone / 50 °C

5: ammonium acetate / methanol / 70 °C

With pyridine; ammonium acetate; hydrogen sulfide; potassium carbonate; triethylamine; In pyridine; methanol; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm00101a017