N-<(1R,4S,5S,6S,8R,9S)-5-Iod-2-oxo-3-oxatricyclo<4.2.1.0^4,8>non-9-ylcarbonyl>-(S)-prolin-benzylester

Base Information

• Chemical Name: N-<(1R,4S,5S,6S,8R,9S)-5-Iod-2-oxo-3-oxatricyclo<4.2.1.0^4,8>non-9-ylcarbonyl>-(S)-prolin-benzylester
• CAS No.: 126255-92-3
• Molecular Formula: C₂₁H₂₂INO₅
• Molecular Weight: 495.314

Synonyms:N-<(1R,4S,5S,6S,8R,9S)-5-Iod-2-oxo-3-oxatricyclo<4.2.1.0^4,8>non-9-ylcarbonyl>-(S)-prolin-benzylester

Chemical Property of N-<(1R,4S,5S,6S,8R,9S)-5-Iod-2-oxo-3-oxatricyclo<4.2.1.0^4,8>non-9-ylcarbonyl>-(S)-prolin-benzylester

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Technology Process of N-<(1R,4S,5S,6S,8R,9S)-5-Iod-2-oxo-3-oxatricyclo<4.2.1.0^4,8>non-9-ylcarbonyl>-(S)-prolin-benzylester

There total 2 articles about N-<(1R,4S,5S,6S,8R,9S)-5-Iod-2-oxo-3-oxatricyclo<4.2.1.0^4,8>non-9-ylcarbonyl>-(S)-prolin-benzylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

N,N'-<(1R,2R,3R,4S)-Bicyclo<2.2.1>hept-5-en-2,3-diyldicarbonyl>-bis<(S)-prolin-benzylester> (126255-88-7) → (S)-1-((1S,3S,6R,7R,9S)-2-Iodo-5-oxo-4-oxa-tricyclo[4.2.1.03,7]nonane-9-carbonyl)-pyrrolidine-2-carboxylic acid benzyl ester (126255-92-3)

Guidance literature:

With iodine; In 1,2-dimethoxyethane; water;

DOI:10.1016/S0040-4039(01)80696-1

Reference yield: 93.0%

N,N'-<(1R,2R,3R,4S)-Bicyclo<2.2.1>hept-5-en-2,3-diyldicarbonyl>-bis<(S)-prolin-benzylester> (126255-88-7) → N-<(1R,4S,5S,6S,8R,9S)-5-Iod-2-oxo-3-oxatricyclo<4.2.1.04,8>non-9-ylcarbonyl>-(S)-prolin-benzylester (126255-92-3)

Guidance literature:

With iodine; In 1,2-dimethoxyethane; water; for 48h; Ambient temperature;

Reference yield: 95.0%

N-<(1R,4S,5S,6S,8R,9S)-5-Iod-2-oxo-3-oxatricyclo<4.2.1.04,8>non-9-ylcarbonyl>-(S)-prolin-benzylester (126255-92-3) → N-<(1R,4S,6S,8R,9S)-2-Oxo-3-oxatricyclo<4.2.1.04,8>non-9-ylcarbonyl>-(S)-prolin-benzylester (126255-93-4)

Guidance literature:

With hydrogen; triethylamine; palladium on activated charcoal; In ethanol; for 48h;

upstream raw materials:

N,N'-<(1R,2R,3R,4S)-Bicyclo<2.2.1>hept-5-en-2,3-diyldicarbonyl>-bis<(S)-prolin-benzylester>

Downstream raw materials:

N-<(1R,4S,6S,8R,9S)-2-Oxo-3-oxatricyclo<4.2.1.0^4,8>non-9-ylcarbonyl>-(S)-prolin-benzylester

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