3-amino-4-(p-chlorophenyl)-5-oxothieno[2,3-b]indeno[2,1-e]pyridine-2-carbo-hydrazide

Base Information

Chemical Name:3-amino-4-(p-chlorophenyl)-5-oxothieno[2,3-b]indeno[2,1-e]pyridine-2-carbo-hydrazide
CAS No.:311767-86-9
Molecular Formula:C₂₁H₁₃ClN₄O₂S
Molecular Weight:420.879
Hs Code.:

Synonyms:3-amino-4-(p-chlorophenyl)-5-oxothieno[2,3-b]indeno[2,1-e]pyridine-2-carbo-hydrazide

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Chemical Property of 3-amino-4-(p-chlorophenyl)-5-oxothieno[2,3-b]indeno[2,1-e]pyridine-2-carbo-hydrazide

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Technology Process of 3-amino-4-(p-chlorophenyl)-5-oxothieno[2,3-b]indeno[2,1-e]pyridine-2-carbo-hydrazide

There total 4 articles about 3-amino-4-(p-chlorophenyl)-5-oxothieno[2,3-b]indeno[2,1-e]pyridine-2-carbo-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 311767-79-0
ethyl 3-amino-4-(p-chlorophenyl)-5-oxothieno[2,3-b]indeno[2,1-e]pyridine-2-carboxylate

: 311767-86-9
3-amino-4-(p-chlorophenyl)-5-oxothieno[2,3-b]indeno[2,1-e]pyridine-2-carbo-hydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 3h; Heating;
DOI:10.1080/00397910008086945

Reference yield:

: 606-23-5
1H-indene-1,3(2H)-dione

: 311767-86-9
3-amino-4-(p-chlorophenyl)-5-oxothieno[2,3-b]indeno[2,1-e]pyridine-2-carbo-hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / piperidine / dioxane / 5 h / Heating

2: 80 percent / sodium ethoxide / ethanol / 1 h / Heating

3: 90 percent / hydrazine hydrate / ethanol / 3 h / Heating

With piperidine; sodium ethanolate; hydrazine hydrate; In 1,4-dioxane; ethanol; 1: Cyclization / 2: cyclocondensation / 3: Substitution;
DOI:10.1080/00397910008086945

Reference yield:

: 68029-53-8
(E)-3-(4-chlorophenyl)-2-cyanoprop-2-enethioamide

: 311767-86-9
3-amino-4-(p-chlorophenyl)-5-oxothieno[2,3-b]indeno[2,1-e]pyridine-2-carbo-hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / piperidine / dioxane / 5 h / Heating

2: 80 percent / sodium ethoxide / ethanol / 1 h / Heating

3: 90 percent / hydrazine hydrate / ethanol / 3 h / Heating

With piperidine; sodium ethanolate; hydrazine hydrate; In 1,4-dioxane; ethanol; 1: Cyclization / 2: cyclocondensation / 3: Substitution;
DOI:10.1080/00397910008086945