2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl 2,3-di-O-benzyl-6-deoxy-α-D-glucopyranoside

Base Information

• Chemical Name: 2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl 2,3-di-O-benzyl-6-deoxy-α-D-glucopyranoside
• CAS No.: 216572-25-7
• Molecular Formula: C₄₀H₄₆O₉
• Molecular Weight: 670.8

Synonyms:2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl 2,3-di-O-benzyl-6-deoxy-α-D-glucopyranoside

Chemical Property of 2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl 2,3-di-O-benzyl-6-deoxy-α-D-glucopyranoside

Chemical Property:

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Technology Process of 2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl 2,3-di-O-benzyl-6-deoxy-α-D-glucopyranoside

There total 4 articles about 2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl 2,3-di-O-benzyl-6-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

2,3-di-O-benzyl-6-deoxy-6-iodo-α-D-glucopyranosyl 2,3-di-O-benzyl-6-deoxy-6-iodo-α-D-glucopyranoside → 2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl 2,3-di-O-benzyl-6-deoxy-α-D-glucopyranoside (216572-25-7)

Guidance literature:

With hydrogen; diethylamine; 10% palladium on active carbon; In ethyl acetate; at 20 ℃; for 24h;

DOI:10.1080/07328309808001900

Reference yield:

2,3,2',3'-tetra-O-benzyl-α,α-trehalose (41548-15-6,93636-47-6,129314-51-8,38992-91-5) → 2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl 2,3-di-O-benzyl-6-deoxy-α-D-glucopyranoside (216572-25-7)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 0 - 20 °C

2: LiAlH₄ / tetrahydrofuran / Heating

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran;

DOI:10.1021/ol026095m

Reference yield:

2,3,2',3'-tetra-O-benzyl-6,6'-di-O-p-tolylsulfonyl-α,α-trehalose (39021-77-7) → 2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl 2,3-di-O-benzyl-6-deoxy-α-D-glucopyranoside (216572-25-7)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; Heating;

DOI:10.1021/ol026095m

upstream raw materials:

2,3,2',3'-tetra-O-benzyl-6,6'-di-O-p-tolylsulfonyl-α,α-trehalose

2,3,2',3'-tetra-O-benzyl-α,α-trehalose

2,3,2',3'-tetra-O-benzyl-4,6;4',6'-di-O-benzylidene-α,α-D-trehalose

Downstream raw materials:

2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl-(1-4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl-(1-4)-2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl 2,3-di-O-benzyl-6-deoxy-α-D-glucopyranoside

4-azido-2,3-di-O-benzyl-4,6-dideoxy-α-D-galactopyranosyl-[1->1]-4-azido-2,3-di-O-behzyl-4,6-dideoxy-α-D-galactopyranoside

4,4'-diazido-2,2'3,3'-tetra-O-benzyl-4,4',6,6'-tetradeoxy-α-D-trehalose

2,3-di-O-benzyl-6-deoxy-α-D-galactopyranosyl-[1->1]-2,3-di-O-benzyl-6-deoxy-α-D-galactopyranoside

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