C₂₃H₃₃NOS

Base Information

• Chemical Name: C₂₃H₃₃NOS
• CAS No.: 1256155-34-6
• Molecular Formula: C₂₃H₃₃NOS
• Molecular Weight: 371.587
• Mol file: 1256155-34-6.mol

Synonyms:C₂₃H₃₃NOS

Chemical Property of C₂₃H₃₃NOS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₃₃NOS

There total 2 articles about C₂₃H₃₃NOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.3%

C18H29NO2 (1256155-28-8) + [(thien-2-yl)methyl]triphenylphosphonium chloride (3462-99-5) → C23H33NOS (1256155-34-6)

Guidance literature:

With phenyllithium; In tetrahydrofuran; dibutyl ether; at 0 ℃; for 2h;

DOI:10.1016/j.tetlet.2010.08.060

Reference yield:

→ C23H33NOS (1256155-34-6)

Guidance literature:

Reference yield: 69.2%

C23H33NOS (1256155-34-6) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → C24H33NO2S (1256155-35-7)

Guidance literature:

C₂₃H₃₃NOS; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

N,N-dimethyl-formamide; In tetrahydrofuran; hexane; at -78 - 20 ℃;

DOI:10.1016/j.tetlet.2010.08.060

upstream raw materials:

C₁₈H₂₉NO₂

[(thien-2-yl)methyl]triphenylphosphonium chloride

Downstream raw materials:

C₂₄H₃₃NO₂S

Refernces

• 1、 Zhang, Xianmin,Aoki, Isao,Piao, Xianqing,Inoue, Shinichiro,Tazawa, Hidehisa,Yokoyama, Shiyoshi,Otomo, Akira. "Effect of modified donor units on molecular hyperpolarizability of thienyl-vinylene nonlinear optical chromophores". supporting information; experimental part. p. 5873 - 5876. Retrieved 2010/12/19.