5,11,17,23-tetra-tert-butyl-25,27-di{2-[4-(2-aminoethoxy)phenoxy]ethoxy}-26,28-dihydroxycalix[4]arene

Base Information

Chemical Name:5,11,17,23-tetra-tert-butyl-25,27-di{2-[4-(2-aminoethoxy)phenoxy]ethoxy}-26,28-dihydroxycalix[4]arene
CAS No.:943857-87-2
Molecular Formula:C₆₄H₈₂N₂O₈
Molecular Weight:1007.36
Hs Code.:

Synonyms:5,11,17,23-tetra-tert-butyl-25,27-di{2-[4-(2-aminoethoxy)phenoxy]ethoxy}-26,28-dihydroxycalix[4]arene

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Chemical Property of 5,11,17,23-tetra-tert-butyl-25,27-di{2-[4-(2-aminoethoxy)phenoxy]ethoxy}-26,28-dihydroxycalix[4]arene

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Technology Process of 5,11,17,23-tetra-tert-butyl-25,27-di{2-[4-(2-aminoethoxy)phenoxy]ethoxy}-26,28-dihydroxycalix[4]arene

There total 5 articles about 5,11,17,23-tetra-tert-butyl-25,27-di{2-[4-(2-aminoethoxy)phenoxy]ethoxy}-26,28-dihydroxycalix[4]arene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 943857-86-1
5,11,17,23-tetra-tert-butyl-25,27-di{2-[4-(2-phthalimidoethoxy)phenoxy]ethoxy}-26,28-dihydroxycalix[4]arene

: 943857-87-2
5,11,17,23-tetra-tert-butyl-25,27-di{2-[4-(2-aminoethoxy)phenoxy]ethoxy}-26,28-dihydroxycalix[4]arene

Guidance literature:: With hydrazine hydrate; In ethanol; for 16h; Heating;
DOI:10.1002/chem.200700041

Reference yield:

: 943857-84-9
2-(4-(2-hydroxyethoxy)phenoxy)ethyl 4-methylbenzenesulfonate

: 943857-87-2
5,11,17,23-tetra-tert-butyl-25,27-di{2-[4-(2-aminoethoxy)phenoxy]ethoxy}-26,28-dihydroxycalix[4]arene

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / dimethylformamide / 16 h / 100 °C

2: 97 percent / DMAP; triethylamine / CH₂Cl₂ / 16 h

3: 75 percent / potassium carbonate / acetonitrile / 96 h / Heating

4: 98 percent / hydrazine monohydrate / ethanol / 16 h / Heating

With dmap; potassium carbonate; hydrazine hydrate; triethylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.200700041

Reference yield:

: 943857-85-0
(2-hydroxylethoxy)-4-(2-phthalimidoethoxy)benzene

: 943857-87-2
5,11,17,23-tetra-tert-butyl-25,27-di{2-[4-(2-aminoethoxy)phenoxy]ethoxy}-26,28-dihydroxycalix[4]arene

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / DMAP; triethylamine / CH₂Cl₂ / 16 h

2: 75 percent / potassium carbonate / acetonitrile / 96 h / Heating

3: 98 percent / hydrazine monohydrate / ethanol / 16 h / Heating

With dmap; potassium carbonate; hydrazine hydrate; triethylamine; In ethanol; dichloromethane; acetonitrile;
DOI:10.1002/chem.200700041