1-<(trichloroethoxy)carbonyl>-2β-(m-methoxybenzyl)-3,4β-epoxypyrrolidine

Base Information

Chemical Name:1-<(trichloroethoxy)carbonyl>-2β-(m-methoxybenzyl)-3,4β-epoxypyrrolidine
CAS No.:84109-99-9
Molecular Formula:C₁₅H₁₆Cl₃NO₄
Molecular Weight:380.655
Hs Code.:

Synonyms:1-<(trichloroethoxy)carbonyl>-2β-(m-methoxybenzyl)-3,4β-epoxypyrrolidine

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Chemical Property of 1-<(trichloroethoxy)carbonyl>-2β-(m-methoxybenzyl)-3,4β-epoxypyrrolidine

Chemical Property:

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Technology Process of 1-<(trichloroethoxy)carbonyl>-2β-(m-methoxybenzyl)-3,4β-epoxypyrrolidine

There total 3 articles about 1-<(trichloroethoxy)carbonyl>-2β-(m-methoxybenzyl)-3,4β-epoxypyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84110-08-7
(2R,3R,4R)-4-Hydroxy-3-iodo-2-(3-methoxy-benzyl)-pyrrolidine-1-carboxylic acid 2,2,2-trichloro-ethyl ester

: 84109-99-9
1-<(trichloroethoxy)carbonyl>-2β-(m-methoxybenzyl)-3,4β-epoxypyrrolidine

Guidance literature:: With potassium hydroxide; In ethanol; for 0.5h; Yield given;
DOI:10.1021/jm00358a003

Reference yield:

: 84109-92-2
2-(m-methoxybenzyl)-3-pyrroline

: 84109-99-9
1-<(trichloroethoxy)carbonyl>-2β-(m-methoxybenzyl)-3,4β-epoxypyrrolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / 2N NaOH / toluene / 1 h / 3 - 5 °C

2: 70percent perchloric acid, N-iodosuccinimide / tetrahydrofuran; H₂O / 1 h / 3 - 25 °C

3: 5percent KOH / ethanol / 0.5 h

With potassium hydroxide; sodium hydroxide; N-iodo-succinimide; perchloric acid; In tetrahydrofuran; ethanol; water; toluene;
DOI:10.1021/jm00358a003

Reference yield:

: 84109-96-6
1-<(trichloroethoxy)carbonyl>-2-(m-methoxybenzyl)-3-pyrroline

: 84109-99-9
1-<(trichloroethoxy)carbonyl>-2β-(m-methoxybenzyl)-3,4β-epoxypyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 70percent perchloric acid, N-iodosuccinimide / tetrahydrofuran; H₂O / 1 h / 3 - 25 °C

2: 5percent KOH / ethanol / 0.5 h

With potassium hydroxide; N-iodo-succinimide; perchloric acid; In tetrahydrofuran; ethanol; water;
DOI:10.1021/jm00358a003