2,8,14-(3',5'-di-tert-butyl-4'-hydroxyphenyl)tribenzotrisdehydro<12>annulene

Base Information

Chemical Name:2,8,14-(3',5'-di-tert-butyl-4'-hydroxyphenyl)tribenzotrisdehydro<12>annulene
CAS No.:221284-76-0
Molecular Formula:C₆₆H₇₂O₃
Molecular Weight:913.296
Hs Code.:

Synonyms:2,8,14-(3',5'-di-tert-butyl-4'-hydroxyphenyl)tribenzotrisdehydro<12>annulene

Suppliers and Price of 2,8,14-(3',5'-di-tert-butyl-4'-hydroxyphenyl)tribenzotrisdehydro<12>annulene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,8,14-(3',5'-di-tert-butyl-4'-hydroxyphenyl)tribenzotrisdehydro<12>annulene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,8,14-(3',5'-di-tert-butyl-4'-hydroxyphenyl)tribenzotrisdehydro<12>annulene

There total 2 articles about 2,8,14-(3',5'-di-tert-butyl-4'-hydroxyphenyl)tribenzotrisdehydro<12>annulene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 4-[3',5'-di-tert-butyl-4'-(trimethylsilyloxy)phenyl]-2-iodo-ethynylbenzene

: 221284-76-0
2,8,14-(3',5'-di-tert-butyl-4'-hydroxyphenyl)tribenzotrisdehydro<12>annulene

Guidance literature:: 4-[3',5'-di-tert-butyl-4'-(trimethylsilyloxy)phenyl]-2-iodo-ethynylbenzene; With ammonium hydroxide; copper(l) chloride; In ethanol; at 20 ℃; for 2.5h;

In pyridine; for 10h; Heating;
DOI:10.1021/jo990575i

Reference yield:

: 221284-74-8
3,5-di-tert-butyl-4'-ethynyl-3'-iodo-biphenyl-4-ol

: 221284-76-0
2,8,14-(3',5'-di-tert-butyl-4'-hydroxyphenyl)tribenzotrisdehydro<12>annulene

Guidance literature:: With ammonium hydroxide; copper(l) chloride; Multistep reaction; 1.) EtOH, r.t., 3-5 h; 2.) pyridine, 90 deg C, 7-10 h;
DOI:10.1246/cl.1999.161