ethyl 4-{[({2-[({[3-(methylthio)phenyl]methyl}amino)carbonyl]-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-5-yl}methyl)oxy]methyl}benzoate

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Chemical Name:ethyl 4-{[({2-[({[3-(methylthio)phenyl]methyl}amino)carbonyl]-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-5-yl}methyl)oxy]methyl}benzoate
CAS No.:869297-06-3
Molecular Formula:C₂₆H₂₅N₃O₅S₂
Molecular Weight:523.634
Hs Code.:

Synonyms:ethyl 4-{[({2-[({[3-(methylthio)phenyl]methyl}amino)carbonyl]-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-5-yl}methyl)oxy]methyl}benzoate

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Chemical Property of ethyl 4-{[({2-[({[3-(methylthio)phenyl]methyl}amino)carbonyl]-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-5-yl}methyl)oxy]methyl}benzoate

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Technology Process of ethyl 4-{[({2-[({[3-(methylthio)phenyl]methyl}amino)carbonyl]-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-5-yl}methyl)oxy]methyl}benzoate

There total 7 articles about ethyl 4-{[({2-[({[3-(methylthio)phenyl]methyl}amino)carbonyl]-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-5-yl}methyl)oxy]methyl}benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 869297-03-0
ethyl 5-{[({4-[(ethyloxy)carbonyl]phenyl}methyl)oxy]methyl}-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidine-2-carboxylate

: 1-[3-(methylthio)phenyl]methanamine hydrochloride

: 869297-06-3
ethyl 4-{[({2-[({[3-(methylthio)phenyl]methyl}amino)carbonyl]-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-5-yl}methyl)oxy]methyl}benzoate

Guidance literature:: With triethylamine; In ethanol; at 80 ℃; for 15h;

Reference yield:

: 869299-71-8
5-({[(4-carboxyphenyl)methyl]oxy}methyl)-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidine-2-carboxylic acid

: 869297-06-3
ethyl 4-{[({2-[({[3-(methylthio)phenyl]methyl}amino)carbonyl]-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-5-yl}methyl)oxy]methyl}benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / tetrahydrofuran / 1 h / 10 - 35 °C

2: pyridine / tetrahydrofuran / 12 h / 10 - 35 °C

3: triethylamine / ethanol / 15 h / 80 °C

With pyridine; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; ethanol;

Reference yield:

: C₁₆H₁₀Cl₂N₂O₄S

: 869297-06-3
ethyl 4-{[({2-[({[3-(methylthio)phenyl]methyl}amino)carbonyl]-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-5-yl}methyl)oxy]methyl}benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / tetrahydrofuran / 12 h / 10 - 35 °C

2: triethylamine / ethanol / 15 h / 80 °C

With pyridine; triethylamine; In tetrahydrofuran; ethanol;