1,1'-(4,5α-epoxy-3,6-dimethoxy-17-methyl-6α,14α-etheno-morphinane-7α,8α-diyl)-bis-ethanone

Base Information

• Chemical Name: 1,1'-(4,5α-epoxy-3,6-dimethoxy-17-methyl-6α,14α-etheno-morphinane-7α,8α-diyl)-bis-ethanone
• CAS No.: 54169-78-7
• Molecular Formula: C₂₅H₂₉NO₅
• Molecular Weight: 423.509

Synonyms:1,1'-(4,5α-epoxy-3,6-dimethoxy-17-methyl-6α,14α-etheno-morphinane-7α,8α-diyl)-bis-ethanone

Chemical Property of 1,1'-(4,5α-epoxy-3,6-dimethoxy-17-methyl-6α,14α-etheno-morphinane-7α,8α-diyl)-bis-ethanone

Chemical Property:

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Technology Process of 1,1'-(4,5α-epoxy-3,6-dimethoxy-17-methyl-6α,14α-etheno-morphinane-7α,8α-diyl)-bis-ethanone

There total 1 articles about 1,1'-(4,5α-epoxy-3,6-dimethoxy-17-methyl-6α,14α-etheno-morphinane-7α,8α-diyl)-bis-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(Z)-hex-3-ene-2,5-dione (17559-81-8) + thebaine (115-37-7) → 1,1'-(4,5α-epoxy-3,6-dimethoxy-17-methyl-6α,14α-etheno-morphinane-7α,8α-diyl)-bis-ethanone (54169-76-5) + 1,1'-(4,5α-epoxy-3,6-dimethoxy-17-methyl-6α,14α-etheno-morphinane-7α,8α-diyl)-bis-ethanone (54169-78-7)

Guidance literature:

In toluene; for 46h; Heating;

DOI:10.1016/S0040-4020(01)97290-4

Reference yield:

phenethylmagnesium bromide (3277-89-2) + 1,1'-(4,5α-epoxy-3,6-dimethoxy-17-methyl-6α,14α-etheno-morphinane-7α,8α-diyl)-bis-ethanone (54169-78-7) → 1-[4,5α-epoxy-7β-((Ξ)-1-hydroxy-1-methyl-3-phenyl-propyl)-3,6-dimethoxy-17-methyl-6α,14α-etheno-morphinan-8α-yl]-ethanone (54169-79-8)

Guidance literature:

In benzene; for 4h; Heating;

DOI:10.1016/S0040-4020(01)97290-4

Reference yield:

phenylmagnesium bromide + 1,1'-(4,5α-epoxy-3,6-dimethoxy-17-methyl-6α,14α-etheno-morphinane-7α,8α-diyl)-bis-ethanone (54169-78-7) → 1-[4,5α-epoxy-7β-((Ξ)-1-hydroxy-1-phenyl-ethyl)-3,6-dimethoxy-17-methyl-6α,14α-etheno-morphinan-8α-yl]-ethanone (54169-75-4)

Guidance literature:

In diethyl ether; for 3.5h; Heating;

DOI:10.1016/S0040-4020(01)97290-4

upstream raw materials:

(Z)-hex-3-ene-2,5-dione

thebaine

Downstream raw materials:

1-[4,5α-epoxy-7β-((Ξ)-1-hydroxy-1-methyl-3-phenyl-propyl)-3,6-dimethoxy-17-methyl-6α,14α-etheno-morphinan-8α-yl]-ethanone

1-[4,5α-epoxy-7β-((Ξ)-1-hydroxy-1-phenyl-ethyl)-3,6-dimethoxy-17-methyl-6α,14α-etheno-morphinan-8α-yl]-ethanone

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