1,4-Bis-<3-(4-fluor-phenyl)-6-ethoxycarbonyl-5-oxo-cyclohex-3-enyl>-benzol

Base Information

Chemical Name:1,4-Bis-<3-(4-fluor-phenyl)-6-ethoxycarbonyl-5-oxo-cyclohex-3-enyl>-benzol
CAS No.:6995-57-9
Molecular Formula:C₃₆H₃₂F₂O₆
Molecular Weight:598.643
Hs Code.:

Synonyms:1,4-Bis-<3-(4-fluor-phenyl)-6-ethoxycarbonyl-5-oxo-cyclohex-3-enyl>-benzol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4-Bis-<3-(4-fluor-phenyl)-6-ethoxycarbonyl-5-oxo-cyclohex-3-enyl>-benzol

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Technology Process of 1,4-Bis-<3-(4-fluor-phenyl)-6-ethoxycarbonyl-5-oxo-cyclohex-3-enyl>-benzol

There total 3 articles about 1,4-Bis-<3-(4-fluor-phenyl)-6-ethoxycarbonyl-5-oxo-cyclohex-3-enyl>-benzol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 6995-56-8
Terephthalbis(p-fluoroacetophenone)

: 141-97-9
ethyl acetoacetate

: 6995-57-9
1,4-Bis-<3-(4-fluor-phenyl)-6-ethoxycarbonyl-5-oxo-cyclohex-3-enyl>-benzol

Guidance literature:: With sodium ethanolate; In ethanol; at 70 - 80 ℃; for 3h;
DOI:10.3109/14756366.2010.530263

Reference yield:

: 623-27-8
terephthalaldehyde,

: 403-42-9
1-(4-fluorophenyl)ethanone

: 6995-57-9
1,4-Bis-<3-(4-fluor-phenyl)-6-ethoxycarbonyl-5-oxo-cyclohex-3-enyl>-benzol

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / ethanol / 4 h / 0 °C

2: sodium ethanolate / ethanol / 3 h / 70 - 80 °C

With sodium ethanolate; sodium hydroxide; In ethanol; 1: Claisen-Schmidt condensation;
DOI:10.3109/14756366.2010.530263

Reference yield:

: 6995-57-9
1,4-Bis-<3-(4-fluor-phenyl)-6-ethoxycarbonyl-5-oxo-cyclohex-3-enyl>-benzol

Guidance literature:: 1,4-Bis-<3-(4-fluor-phenyl)-3-oxo-prop-1-enyl>-benzol, aus Natrium und Acetessigsaeure-ethylester in A. bereitete Lsg., Erwaermen;

upstream raw materials:

Terephthalbis(p-fluoroacetophenone)

ethyl acetoacetate

terephthalaldehyde,

1-(4-fluorophenyl)ethanone

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