6,7-dichloro-2-methyl-2-phenyl-5-trifluoromethylsulfonyloxy-1-indanone

Base Information

• Chemical Name: 6,7-dichloro-2-methyl-2-phenyl-5-trifluoromethylsulfonyloxy-1-indanone
• CAS No.: 71500-91-9
• Molecular Formula: C₁₇H₁₁Cl₂F₃O₄S
• Molecular Weight: 439.239

Synonyms:6,7-dichloro-2-methyl-2-phenyl-5-trifluoromethylsulfonyloxy-1-indanone

Chemical Property of 6,7-dichloro-2-methyl-2-phenyl-5-trifluoromethylsulfonyloxy-1-indanone

Chemical Property:

Purity/Quality:

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Technology Process of 6,7-dichloro-2-methyl-2-phenyl-5-trifluoromethylsulfonyloxy-1-indanone

There total 3 articles about 6,7-dichloro-2-methyl-2-phenyl-5-trifluoromethylsulfonyloxy-1-indanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

trifluoromethane sulfonyl chloride (421-83-0) + 6,7-dichloro-2,3-dihydro-5-hydroxy-2-methyl-2-phenyl-1H-inden-1-one (57509-50-9,76640-83-0,76640-84-1) → 6,7-dichloro-2-methyl-2-phenyl-5-trifluoromethylsulfonyloxy-1-indanone (71500-91-9)

Guidance literature:

In acetone; in presence of K2CO3, at 20°C, ca. 1 h;

DOI:10.1021/jo01337a008

Reference yield:

trifluoromethane sulfonyl chloride (421-83-0) + 6,7-dichloro-2,3-dihydro-5-hydroxy-2-methyl-2-phenyl-1H-inden-1-one (57509-50-9,76640-83-0,76640-84-1) → 6,7-dichloro-2-methyl-2-phenyl-5-trifluoromethylsulfonyloxy-1-indanone (71500-91-9) + (6,7-dichloro-1-oxo-2-methyl-2-phenyl-5-indanyl)acetic acid (71500-88-4)

Guidance literature:

With potassium carbonate; In acetone;

Reference yield:

→ 6,7-dichloro-2-methyl-2-phenyl-5-trifluoromethylsulfonyloxy-1-indanone (71500-91-9)

Guidance literature:

Hydroxyindanon 3c, Trifluormethansulfonylchlorid;

DOI:10.1021/jo01337a008

upstream raw materials:

trifluoromethane sulfonyl chloride

6,7-dichloro-2,3-dihydro-5-hydroxy-2-methyl-2-phenyl-1H-inden-1-one

Downstream raw materials:

(6,7-dichloro-1-oxo-2-methyl-2-phenyl-5-indanyl)acetic acid

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