1D-2,4,5,6-O-tetrakis(methoxymethylene)-myo-inositol 3-(dibenzylphosphate)

Base Information

• Chemical Name: 1D-2,4,5,6-O-tetrakis(methoxymethylene)-myo-inositol 3-(dibenzylphosphate)
• CAS No.: 165689-90-7
• Molecular Formula: C₂₈H₄₁O₁₃P
• Molecular Weight: 616.599

Synonyms:1D-2,4,5,6-O-tetrakis(methoxymethylene)-myo-inositol 3-(dibenzylphosphate)

Chemical Property of 1D-2,4,5,6-O-tetrakis(methoxymethylene)-myo-inositol 3-(dibenzylphosphate)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of 1D-2,4,5,6-O-tetrakis(methoxymethylene)-myo-inositol 3-(dibenzylphosphate)

There total 2 articles about 1D-2,4,5,6-O-tetrakis(methoxymethylene)-myo-inositol 3-(dibenzylphosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

1D-1-O-(tert-butyldiphenylsilyl)-2,4,5,6-O-tetrakis(methoxymethylene)-myo-inositol 3-(dibenzyl phosphate) (165689-89-4) → 1D-2,4,5,6-O-tetrakis(methoxymethylene)-myo-inositol 3-(dibenzylphosphate) (165689-90-7)

Guidance literature:

With tetraethylammonium fluoride; In N,N-dimethyl-formamide; for 1h;

DOI:10.1021/jo0206418

Reference yield:

Dibenzyl N,N-diisopropylphosphoramidite (108549-23-1) → 1D-2,4,5,6-O-tetrakis(methoxymethylene)-myo-inositol 3-(dibenzylphosphate) (165689-90-7)

Guidance literature:

Multi-step reaction with 2 steps

1.1: tetrazole / acetonitrile / 6 h

1.2: 81 percent / 3-chloroperoxybenzoic acid / acetonitrile; CHCl₃ / -20 - 20 °C

2.1: 87 percent / tetraethylammonium fluoride / dimethylformamide / 1 h

With 1H-tetrazole; tetraethylammonium fluoride; In N,N-dimethyl-formamide; acetonitrile;

DOI:10.1021/jo0206418

Reference yield:

Hexadecanoic acid (R)-2-(diisopropylamino-methoxy-phosphanyloxy)-1-hexadecanoyloxymethyl-ethyl ester (496808-59-4) + 1D-2,4,5,6-O-tetrakis(methoxymethylene)-myo-inositol 3-(dibenzylphosphate) (165689-90-7) → Hexadecanoic acid (R)-2-{[(1S,2S,3R,4S,5R,6R)-3-(bis-benzyloxy-phosphoryloxy)-2,4,5,6-tetrakis-methoxymethoxy-cyclohexyloxy]-methoxy-phosphanyloxy}-1-hexadecanoyloxymethyl-ethyl ester

Guidance literature:

With 1H-tetrazole;

DOI:10.1021/jo0206418

upstream raw materials:

1D-1-O-(tert-butyldiphenylsilyl)-2,4,5,6-O-tetrakis(methoxymethylene)-myo-inositol 3-(dibenzyl phosphate)

Dibenzyl N,N-diisopropylphosphoramidite

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