2'-oxo-1',3',4,5-tetrahydrospiro[1,3,4-oxadiazole-5,3'-(2'H)-indole]-2-ylacetonitrile

Base Information

Chemical Name:2'-oxo-1',3',4,5-tetrahydrospiro[1,3,4-oxadiazole-5,3'-(2'H)-indole]-2-ylacetonitrile
CAS No.:462101-23-1
Molecular Formula:C₁₁H₈N₄O₂
Molecular Weight:228.21
Hs Code.:

Synonyms:5-cyanomethyl-1,3,4-oxadiazol-(3H)-2-spiro-3-indol-2-(1H)-one

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Chemical Property of 2'-oxo-1',3',4,5-tetrahydrospiro[1,3,4-oxadiazole-5,3'-(2'H)-indole]-2-ylacetonitrile

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Technology Process of 2'-oxo-1',3',4,5-tetrahydrospiro[1,3,4-oxadiazole-5,3'-(2'H)-indole]-2-ylacetonitrile

There total 2 articles about 2'-oxo-1',3',4,5-tetrahydrospiro[1,3,4-oxadiazole-5,3'-(2'H)-indole]-2-ylacetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 29775-72-2
cyano-N'-(2-oxo-1,2-dihydroindol-3-ylidene)acetohydrazide

: 462101-23-1
5-cyanomethyl-1,3,4-oxadiazol-(3H)-2-spiro-3-indol-2-(1H)-one

Guidance literature:: In acetic acid; for 2h; Heating;
DOI:10.1002/hc.10020

Reference yield:

: 91-56-5,1186480-61-4,84788-92-1
indole-2,3-dione

: 462101-23-1
5-cyanomethyl-1,3,4-oxadiazol-(3H)-2-spiro-3-indol-2-(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / ethanol / 1 h / Heating

2: 80 percent / acetic acid / 2 h / Heating

In ethanol; acetic acid;
DOI:10.1002/hc.10020